2,5-bis(1-benzyl-5-(E)-(methoxycarbonyl)methyliminomethyl-1H-pyrrol-2-yl)-thiophene

Base Information

Chemical Name:2,5-bis(1-benzyl-5-(E)-(methoxycarbonyl)methyliminomethyl-1H-pyrrol-2-yl)-thiophene
CAS No.:1006726-71-1
Molecular Formula:C₃₄H₃₂N₄O₄S
Molecular Weight:592.718
Hs Code.:

Synonyms:2,5-bis(1-benzyl-5-(E)-(methoxycarbonyl)methyliminomethyl-1H-pyrrol-2-yl)-thiophene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,5-bis(1-benzyl-5-(E)-(methoxycarbonyl)methyliminomethyl-1H-pyrrol-2-yl)-thiophene

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Technology Process of 2,5-bis(1-benzyl-5-(E)-(methoxycarbonyl)methyliminomethyl-1H-pyrrol-2-yl)-thiophene

There total 1 articles about 2,5-bis(1-benzyl-5-(E)-(methoxycarbonyl)methyliminomethyl-1H-pyrrol-2-yl)-thiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1006726-56-2
2,5-bis(1-benzyl-5-carbaldehyde-1H-pyrrol-2-yl)-thiophene

: 5680-79-5,883886-67-7
glycine ethyl ester hydrochloride

: 1006726-71-1
2,5-bis(1-benzyl-5-(E)-(methoxycarbonyl)methyliminomethyl-1H-pyrrol-2-yl)-thiophene

Guidance literature:: With silica gel; triethylamine; In ethanol; at 20 ℃; for 2.5h;
DOI:10.1002/anie.200703258

Reference yield:

: 1006726-71-1
2,5-bis(1-benzyl-5-(E)-(methoxycarbonyl)methyliminomethyl-1H-pyrrol-2-yl)-thiophene

: 963-16-6
(E)-1,2-bis(phenylsulfonyl)ethylene

: 1006726-81-3
5-[1''-benzyl-5''-formyl-1''H-pyrrol-2''-yl]-2-[1'-benzyl-5-(methoxycarbonyl)-1H,1'H-[2,5']-bipyrrol-2-yl]-thiophene

: 1006726-58-4
2,5-bis[1'-benzyl-5-(methoxycarbonyl)-1H,1'H-[2,2']-bipyrrol-2'-yl]-thiophene

Guidance literature:: 2,5-bis(1-benzyl-5-(E)-(methoxycarbonyl)methyliminomethyl-1H-pyrrol-2-yl)-thiophene; (E)-1,2-bis(phenylsulfonyl)ethylene; With 4 A molecular sieve; triethylamine; triphenylphosphine; tetrakis(actonitrile)copper(I) hexafluorophosphate; In tetrahydrofuran; at 20 ℃; for 5h;

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at 20 ℃; for 0.5h; Further stages.;
DOI:10.1002/anie.200703258