Acetic acid (1S,2R)-1-(4-methoxy-benzyloxymethyl)-2-methyl-pent-4-ynyl ester

Base Information

Chemical Name:Acetic acid (1S,2R)-1-(4-methoxy-benzyloxymethyl)-2-methyl-pent-4-ynyl ester
CAS No.:868150-19-0
Molecular Formula:C₁₇H₂₂O₄
Molecular Weight:290.359
Hs Code.:

Synonyms:Acetic acid (1S,2R)-1-(4-methoxy-benzyloxymethyl)-2-methyl-pent-4-ynyl ester

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Chemical Property of Acetic acid (1S,2R)-1-(4-methoxy-benzyloxymethyl)-2-methyl-pent-4-ynyl ester

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Technology Process of Acetic acid (1S,2R)-1-(4-methoxy-benzyloxymethyl)-2-methyl-pent-4-ynyl ester

There total 2 articles about Acetic acid (1S,2R)-1-(4-methoxy-benzyloxymethyl)-2-methyl-pent-4-ynyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 868150-16-7
(2S,3R)-1-(4-Methoxy-benzyloxy)-3-methyl-hex-5-yn-2-ol

: 108-24-7
acetic anhydride

: 868150-19-0
Acetic acid (1S,2R)-1-(4-methoxy-benzyloxymethyl)-2-methyl-pent-4-ynyl ester

Guidance literature:: With pyridine; at 20 ℃; for 6h;
DOI:10.1021/ja053365y

Reference yield:

: 476452-91-2
(2S,3R)-1-(4-Methoxy-benzyloxy)-3-methyl-6-trimethylsilanyl-hex-5-yn-2-ol

: 868150-19-0
Acetic acid (1S,2R)-1-(4-methoxy-benzyloxymethyl)-2-methyl-pent-4-ynyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / tetrabutylammonium fluoride / tetrahydrofuran / 0.75 h / 20 °C

2: 93 percent / pyridine / 6 h / 20 °C

With pyridine; tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1021/ja053365y

Reference yield:

: 868150-19-0
Acetic acid (1S,2R)-1-(4-methoxy-benzyloxymethyl)-2-methyl-pent-4-ynyl ester

: 868056-82-0
{(2R,3R)-3-[1-((2R,3R)-3-Allyl-1,4-dioxa-spiro[4.4]non-2-yl)-vinyl]-1,4-dioxa-spiro[4.4]non-2-ylethynyl}-trimethyl-silane

: 868150-27-0
(E)-(2S,3R)-8-{(2R,3R)-3-[1-((2R,3R)-3-Ethynyl-1,4-dioxa-spiro[4.4]non-2-yl)-vinyl]-1,4-dioxa-spiro[4.4]non-2-yl}-1-(4-methoxy-benzyloxy)-3-methyl-5-methylene-oct-7-en-2-ol

Guidance literature:: Acetic acid (1S,2R)-1-(4-methoxy-benzyloxymethyl)-2-methyl-pent-4-ynyl ester; {(2R,3R)-3-[1-((2R,3R)-3-Allyl-1,4-dioxa-spiro[4.4]non-2-yl)-vinyl]-1,4-dioxa-spiro[4.4]non-2-ylethynyl}-trimethyl-silane; With cyclopentadienylruthenium(II) trisacetonitrile hexafluorophosphate; In N,N-dimethyl-formamide; at 60 ℃; for 3h;

With barium dihydroxide; In methanol; at 20 ℃; for 1.5h;
DOI:10.1021/ja053365y