Technology Process of C14H17NO3
There total 3 articles about C14H17NO3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
2,6-dimethylpyridine; trifluoroacetic anhydride;
In
toluene;
at 0 ℃;
for 4.5h;
Inert atmosphere;
Reflux;
DOI:10.1016/j.tetlet.2012.01.086
- Guidance literature:
-
Multi-step reaction with 3 steps
1: Grubbs catalyst first generation / dichloromethane / 20 °C / Inert atmosphere
2: water; palladium diacetate / acetonitrile / 0.25 h / 20 °C
3: 2,6-dimethylpyridine; trifluoroacetic anhydride / toluene / 4.5 h / 0 °C / Inert atmosphere; Reflux
With
2,6-dimethylpyridine; Grubbs catalyst first generation; water; palladium diacetate; trifluoroacetic anhydride;
In
dichloromethane; toluene; acetonitrile;
DOI:10.1016/j.tetlet.2012.01.086
- Guidance literature:
-
Multi-step reaction with 2 steps
1: water; palladium diacetate / acetonitrile / 0.25 h / 20 °C
2: 2,6-dimethylpyridine; trifluoroacetic anhydride / toluene / 4.5 h / 0 °C / Inert atmosphere; Reflux
With
2,6-dimethylpyridine; water; palladium diacetate; trifluoroacetic anhydride;
In
toluene; acetonitrile;
DOI:10.1016/j.tetlet.2012.01.086