3'-O-azidomethyl-N⁴-benzoyl-2',5'-bis-O-tert-butyldimethylsilylcytidine

Base Information

Chemical Name:3'-O-azidomethyl-N⁴-benzoyl-2',5'-bis-O-tert-butyldimethylsilylcytidine
CAS No.:329032-98-6
Molecular Formula:C₂₉H₄₆N₆O₆Si₂
Molecular Weight:630.892
Hs Code.:

3'-O-azidomethyl-N<sup>4</sup>-benzoyl-2',5'-bis-O-tert-butyldimethylsilylcytidine

Synonyms:3'-O-azidomethyl-N⁴-benzoyl-2',5'-bis-O-tert-butyldimethylsilylcytidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3'-O-azidomethyl-N⁴-benzoyl-2',5'-bis-O-tert-butyldimethylsilylcytidine

Chemical Property:

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Technology Process of 3'-O-azidomethyl-N⁴-benzoyl-2',5'-bis-O-tert-butyldimethylsilylcytidine

There total 3 articles about 3'-O-azidomethyl-N⁴-benzoyl-2',5'-bis-O-tert-butyldimethylsilylcytidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N-{1-[3-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-4-chloromethoxy-tetrahydro-furan-2-yl]-2-oxo-1,2-dihydro-pyrimidin-4-yl}-benzamide

: 329032-98-6
3'-O-azidomethyl-N⁴-benzoyl-2',5'-bis-O-tert-butyldimethylsilylcytidine

Guidance literature:: With lithium azide; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;
DOI:10.1080/15257770008045472

Reference yield:

: N-{1-[4-bromomethoxy-3-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-tetrahydro-furan-2-yl]-2-oxo-1,2-dihydro-pyrimidin-4-yl}-benzamide

: 329032-98-6
3'-O-azidomethyl-N⁴-benzoyl-2',5'-bis-O-tert-butyldimethylsilylcytidine

Guidance literature:: With lithium azide; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;
DOI:10.1080/15257770008045472

Reference yield:

: 292042-79-6
N-{1-[3-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-4-methylsulfanylmethoxy-tetrahydro-furan-2-yl]-2-oxo-1,2-dihydro-pyrimidin-4-yl}-benzamide

: 329032-98-6
3'-O-azidomethyl-N⁴-benzoyl-2',5'-bis-O-tert-butyldimethylsilylcytidine

Guidance literature:: Multi-step reaction with 2 steps

1: SO₂Cl₂ / 1,2-dichloro-ethane / 0 °C

2: 214 mg / LiN₃ / dimethylformamide / 0.5 h / 20 °C

With sulfuryl dichloride; lithium azide; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1080/15257770008045472