tetraphenylarsonium tetrachlorooxotechnetate(V)

Base Information

Chemical Name:tetraphenylarsonium tetrachlorooxotechnetate(V)
CAS No.:85129-39-1
Molecular Formula:C₂₄H₂₀As*Cl₄OTc
Molecular Weight:639.063
Hs Code.:

Synonyms:tetraphenylarsonium tetrachlorooxotechnetate(V)

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Chemical Property of tetraphenylarsonium tetrachlorooxotechnetate(V)

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Technology Process of tetraphenylarsonium tetrachlorooxotechnetate(V)

There total 2 articles about tetraphenylarsonium tetrachlorooxotechnetate(V) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: tetraphenylarsonium pertechnetate

: 85129-39-1
tetraphenylarsonium tetrachlorooxotechnetate

Guidance literature:: With SOCl₂; In thionyl chloride; standing 2.5h at room temp.; drying on a rotary evaporator, suspending in abs.ethanol, filtration, washing with abs.ethanol; elem.anal.;

Reference yield:

: 34035-97-7
ammonium pertechnetate

: 507-28-8,14842-08-1
tetraphenylarsonium chloride

: 85129-39-1
tetraphenylarsonium tetrachlorooxotechnetate(V)

Guidance literature:: In hydrogenchloride; addn. of 2 equiv. of As-compd. to NH4TcO4 (in 12 M HCl), stirring (room temp., 30 min, pptn.); filtration, washing (12M HCl, 2-PrOH/Et2O=4:6);
DOI:10.1021/ic951030j

Reference yield: 91.0%

: 85129-39-1
tetraphenylarsonium tetrachlorooxotechnetate

: 507-28-8,14842-08-1
tetraphenylarsonium chloride

: {AsPh₄}2{TcCl₆}

Guidance literature:: With SOCl₂; In thionyl chloride; heating under reflux for 5 min.; evapn. to dryness on a rotary evaporator, extraction with abs.ethanol, removing of excess As(C6H5)4Cl, filtration, washing with abs.ethanol, elem. anal.;