(Z)-4-hydroxy-3-{1-[2-(2-methoxybenzoyl)hydrazono]ethyl}phenethyl acetate

Base Information

• Chemical Name: (Z)-4-hydroxy-3-{1-[2-(2-methoxybenzoyl)hydrazono]ethyl}phenethyl acetate
• CAS No.: 1322684-82-1
• Molecular Formula: C₂₀H₂₂N₂O₅
• Molecular Weight: 370.405

Synonyms:(Z)-4-hydroxy-3-{1-[2-(2-methoxybenzoyl)hydrazono]ethyl}phenethyl acetate

Chemical Property of (Z)-4-hydroxy-3-{1-[2-(2-methoxybenzoyl)hydrazono]ethyl}phenethyl acetate

Chemical Property:

Purity/Quality:

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Technology Process of (Z)-4-hydroxy-3-{1-[2-(2-methoxybenzoyl)hydrazono]ethyl}phenethyl acetate

There total 2 articles about (Z)-4-hydroxy-3-{1-[2-(2-methoxybenzoyl)hydrazono]ethyl}phenethyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

2-methoxybenzoylhydrazine (7466-54-8) + 3-acetyl-4-hydroxyphenethyl acetate (58282-50-1) → (Z)-4-hydroxy-3-{1-[2-(2-methoxybenzoyl)hydrazono]ethyl}phenethyl acetate (1322684-82-1)

Guidance literature:

In propan-1-ol; for 12h; Reflux;

DOI:10.1246/bcsj.20100340

Reference yield:

2-(4-Methoxyphenyl)ethanol (702-23-8) → (Z)-4-hydroxy-3-{1-[2-(2-methoxybenzoyl)hydrazono]ethyl}phenethyl acetate (1322684-82-1)

Guidance literature:

Multi-step reaction with 2 steps

1: aluminum (III) chloride / 1,1,2,2-tetrachloroethane / 22 h / 0 - 20 °C

2: propan-1-ol / 12 h / Reflux

With aluminum (III) chloride; In propan-1-ol; 1,1,2,2-tetrachloroethane; 1: Fries rearrangement;

DOI:10.1246/bcsj.20100340

Reference yield: 92.0%

(Z)-4-hydroxy-3-{1-[2-(2-methoxybenzoyl)hydrazono]ethyl}phenethyl acetate (1322684-82-1) → 3-acetyl-4-(2-methoxybenzoyl)phenethyl acetate (1322684-83-2)

Guidance literature:

With lead(IV) tetraacetate; In tetrahydrofuran; at 20 ℃; for 2h;

DOI:10.1246/bcsj.20100340

upstream raw materials:

2-(4-Methoxyphenyl)ethanol

2-methoxybenzoylhydrazine

3-acetyl-4-hydroxyphenethyl acetate

Downstream raw materials:

(MeOC₆H₄)(AcOCH₂CH₂)C₈H₄NCHC₈H₃N(CH₂CH₂OH)(C₆H₄OMe)

((MeOC₆H₄)(AcOCH₂CH₂)C₈H₃NCHC₈H₃N(CH₂CH₂OH)(C₆H₄OMe))BF₂

((MeOC₆H₄)(AcOCH₂CH₂)C₈H₃NCHC₈H₃N(CH₂CH₂OCOC(CH₃)CH₂)(C₆H₄OMe))BF₂

3-acetyl-4-(2-methoxybenzoyl)phenethyl acetate

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