methyl β-(4-fluorophenyl)-α-(2-methyl-1-oxopropyl)-2-oxo-3-piperidinepropanoic acid

Base Information

Chemical Name:methyl β-(4-fluorophenyl)-α-(2-methyl-1-oxopropyl)-2-oxo-3-piperidinepropanoic acid
CAS No.:853182-60-2
Molecular Formula:C₁₉H₂₄FNO₄
Molecular Weight:349.402
Hs Code.:

Synonyms:methyl β-(4-fluorophenyl)-α-(2-methyl-1-oxopropyl)-2-oxo-3-piperidinepropanoic acid

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Chemical Property of methyl β-(4-fluorophenyl)-α-(2-methyl-1-oxopropyl)-2-oxo-3-piperidinepropanoic acid

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Technology Process of methyl β-(4-fluorophenyl)-α-(2-methyl-1-oxopropyl)-2-oxo-3-piperidinepropanoic acid

There total 1 articles about methyl β-(4-fluorophenyl)-α-(2-methyl-1-oxopropyl)-2-oxo-3-piperidinepropanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 853182-58-8
methyl 1-[(1,1-dimethylethoxy)carbonyl]-β-(4-fluorophenyl)-α-(2-methyl-1-oxopropyl)-2-oxo-3-piperidinepropanoate

: 853182-60-2
methyl β-(4-fluorophenyl)-α-(2-methyl-1-oxopropyl)-2-oxo-3-piperidinepropanoic acid

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 10 - 20 ℃; for 2h;

Reference yield: 30.0%

: 853182-60-2
methyl β-(4-fluorophenyl)-α-(2-methyl-1-oxopropyl)-2-oxo-3-piperidinepropanoic acid

: 76-05-1
trifluoroacetic acid

: methyl 4-(4-fluorophenyl)-2-isopropyl-5,6,7,8-tetrahydro-[1,8]naphthyridine-3-carboxylate trifluoroacetate

Guidance literature:: methyl β-(4-fluorophenyl)-α-(2-methyl-1-oxopropyl)-2-oxo-3-piperidinepropanoic acid; With phosphorus pentachloride; In 1,1-dichloroethane; at 65 ℃; for 2.5h;

With ammonium acetate; In methanol; at 60 ℃; for 4h;

trifluoroacetic acid; With copper diacetate; more than 3 stages;