C₂₂H₁₄F₆N₂O₃

Base Information

Chemical Name:C₂₂H₁₄F₆N₂O₃
CAS No.:1276040-33-5
Molecular Formula:C₂₂H₁₄F₆N₂O₃
Molecular Weight:468.355
Hs Code.:

C<sub>22</sub>H<sub>14</sub>F<sub>6</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₂₂H₁₄F₆N₂O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₁₄F₆N₂O₃

Chemical Property:

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Technology Process of C₂₂H₁₄F₆N₂O₃

There total 5 articles about C₂₂H₁₄F₆N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 57772-57-3
5-hydroxy-2-iodo-benzoic acid

: 1276040-33-5
C₂₂H₁₄F₆N₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid / 18 h / Reflux

2: potassium carbonate / dimethyl sulfoxide / 1.5 h / 80 - 82 °C

3: caesium carbonate / 4a,9a-dihydro-9,9-dimethyl-4,5-bis(diphenylphosphino)-xanthene; palladium diacetate / toluene / 1.5 h / 60 °C / Inert atmosphere; Sonication

4: water; sodium hydroxide / tetrahydrofuran; methanol / 4 h / 20 °C

With sulfuric acid; water; potassium carbonate; caesium carbonate; sodium hydroxide; 4a,9a-dihydro-9,9-dimethyl-4,5-bis(diphenylphosphino)-xanthene; palladium diacetate; In tetrahydrofuran; methanol; dimethyl sulfoxide; toluene;

Reference yield:

: 1276040-32-4
C₂₃H₁₆F₆N₂O₃

: 1276040-33-5
C₂₂H₁₄F₆N₂O₃

Guidance literature:: C₂₃H₁₆F₆N₂O₃; With water; sodium hydroxide; In tetrahydrofuran; methanol; at 20 ℃; for 4h;

With hydrogenchloride; In tetrahydrofuran; methanol; water;

Reference yield:

: 394-31-0
2-amino-5-hydroxybenzoic acid

: 1276040-33-5
C₂₂H₁₄F₆N₂O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfuric acid; sodium nitrite / water / 0.5 h / 0 - 5 °C

1.2: 1 h / 80 - 90 °C

2.1: sulfuric acid / 18 h / Reflux

3.1: potassium carbonate / dimethyl sulfoxide / 1.5 h / 80 - 82 °C

4.1: caesium carbonate / 4a,9a-dihydro-9,9-dimethyl-4,5-bis(diphenylphosphino)-xanthene; palladium diacetate / toluene / 1.5 h / 60 °C / Inert atmosphere; Sonication

5.1: water; sodium hydroxide / tetrahydrofuran; methanol / 4 h / 20 °C

With sulfuric acid; water; potassium carbonate; caesium carbonate; sodium hydroxide; sodium nitrite; 4a,9a-dihydro-9,9-dimethyl-4,5-bis(diphenylphosphino)-xanthene; palladium diacetate; In tetrahydrofuran; methanol; water; dimethyl sulfoxide; toluene;