Technology Process of C15H19ClO3
There total 5 articles about C15H19ClO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene;
In
dichloromethane;
at 23 ℃;
for 20h;
Inert atmosphere;
DOI:10.1021/ja404578u
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: scandium tris(trifluoromethanesulfonate) / dichloromethane / 2 h / 23 °C / Inert atmosphere
2.1: Schwartz's reagent / toluene / 23 - 50 °C / Inert atmosphere
2.2: 0.5 h / 0 - 23 °C / Inert atmosphere
3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 23 °C / Inert atmosphere
4.1: [bis(acetoxy)iodo]benzene; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane / 20 h / 23 °C / Inert atmosphere
With
Schwartz's reagent; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; tetrabutyl ammonium fluoride; scandium tris(trifluoromethanesulfonate);
In
tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/ja404578u
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 23 °C / Inert atmosphere
2: [bis(acetoxy)iodo]benzene; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane / 20 h / 23 °C / Inert atmosphere
With
2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; tetrabutyl ammonium fluoride;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ja404578u
