1-tert-butyl-3-(1-(4-chlorophenyl)-3-methyl-1-oxobutan-2-yl)-1-methyl urea

Base Information

Chemical Name:1-tert-butyl-3-(1-(4-chlorophenyl)-3-methyl-1-oxobutan-2-yl)-1-methyl urea
CAS No.:1394017-55-0
Molecular Formula:C₁₇H₂₅ClN₂O₂
Molecular Weight:324.851
Hs Code.:

Synonyms:1-tert-butyl-3-(1-(4-chlorophenyl)-3-methyl-1-oxobutan-2-yl)-1-methyl urea

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Chemical Property of 1-tert-butyl-3-(1-(4-chlorophenyl)-3-methyl-1-oxobutan-2-yl)-1-methyl urea

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Technology Process of 1-tert-butyl-3-(1-(4-chlorophenyl)-3-methyl-1-oxobutan-2-yl)-1-methyl urea

There total 4 articles about 1-tert-butyl-3-(1-(4-chlorophenyl)-3-methyl-1-oxobutan-2-yl)-1-methyl urea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 14610-37-8
N-methyl-tert-butylamine

: 1394017-59-4
tert-butyl 1-(4-chlorophenyl)-3-methyl-1-oxobutan-2-ylcarbamate

: 530-62-1
1,1'-carbonyldiimidazole

: 1394017-55-0
1-tert-butyl-3-(1-(4-chlorophenyl)-3-methyl-1-oxobutan-2-yl)-1-methyl urea

Guidance literature:: tert-butyl 1-(4-chlorophenyl)-3-methyl-1-oxobutan-2-ylcarbamate; 1,1'-carbonyldiimidazole; With triethylamine; In acetonitrile; for 0.333333h;

N-methyl-tert-butylamine; In acetonitrile; for 0.5h;

Reference yield:

: 14610-37-8
N-methyl-tert-butylamine

: C₁₅H₁₆ClN₃O₂

: 1394017-55-0
1-tert-butyl-3-(1-(4-chlorophenyl)-3-methyl-1-oxobutan-2-yl)-1-methyl urea

Guidance literature:: In acetonitrile; for 1.5h; Inert atmosphere;
DOI:10.1016/j.bmcl.2012.07.032

Reference yield:

: 1394017-59-4
tert-butyl 1-(4-chlorophenyl)-3-methyl-1-oxobutan-2-ylcarbamate

: 1394017-55-0
1-tert-butyl-3-(1-(4-chlorophenyl)-3-methyl-1-oxobutan-2-yl)-1-methyl urea

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / acetonitrile / 1.5 h / Inert atmosphere

2: acetonitrile / 1.5 h / Inert atmosphere

With triethylamine; In acetonitrile;
DOI:10.1016/j.bmcl.2012.07.032