1-O-allyl-2-O-(2-O-[2-azidomethylbenzoyl]-3,4-di-O-benzyl-6-O-hexadecanoyl-α-D-mannopyranosyl)-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol

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Chemical Name:1-O-allyl-2-O-(2-O-[2-azidomethylbenzoyl]-3,4-di-O-benzyl-6-O-hexadecanoyl-α-D-mannopyranosyl)-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol
CAS No.:1336875-77-4
Molecular Formula:C₁₀₈H₁₂₅N₃O₁₈
Molecular Weight:1753.19
Hs Code.:

1-O-allyl-2-O-(2-O-[2-azidomethylbenzoyl]-3,4-di-O-benzyl-6-O-hexadecanoyl-α-D-mannopyranosyl)-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol

Synonyms:1-O-allyl-2-O-(2-O-[2-azidomethylbenzoyl]-3,4-di-O-benzyl-6-O-hexadecanoyl-α-D-mannopyranosyl)-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol

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Chemical Property of 1-O-allyl-2-O-(2-O-[2-azidomethylbenzoyl]-3,4-di-O-benzyl-6-O-hexadecanoyl-α-D-mannopyranosyl)-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol

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Technology Process of 1-O-allyl-2-O-(2-O-[2-azidomethylbenzoyl]-3,4-di-O-benzyl-6-O-hexadecanoyl-α-D-mannopyranosyl)-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol

There total 1 articles about 1-O-allyl-2-O-(2-O-[2-azidomethylbenzoyl]-3,4-di-O-benzyl-6-O-hexadecanoyl-α-D-mannopyranosyl)-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 1336875-75-2
phenyl 2-O-(2-azidomethylbenzoyl)-3,4-di-O-benzyl-6-O-hexadecanoyl-1-thio-α-D-mannopyranoside

: 132360-52-2,132437-48-0
1-O-allyl-3,4,5-tri-O-benzyl-6-O-(2',3',4',6'-tetra-O-benzyl-α-D-mannopyranosyl)-D-myo-inositol

: 1336875-77-4
1-O-allyl-2-O-(2-O-[2-azidomethylbenzoyl]-3,4-di-O-benzyl-6-O-hexadecanoyl-α-D-mannopyranosyl)-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol

Guidance literature:: phenyl 2-O-(2-azidomethylbenzoyl)-3,4-di-O-benzyl-6-O-hexadecanoyl-1-thio-α-D-mannopyranoside; With 2,6-di-tert-butyl-4-methylpyridine; trifluoromethylsulfonic anhydride; 1,1'-sulfinylbisbenzene; In dichloromethane; at -60 ℃; for 0.0833333h;

1-O-allyl-3,4,5-tri-O-benzyl-6-O-(2',3',4',6'-tetra-O-benzyl-α-D-mannopyranosyl)-D-myo-inositol; In dichloromethane; at -60 - 0 ℃; for 3h;
DOI:10.1021/jm2008419

Reference yield: 82.0%

: 1336875-77-4
1-O-allyl-2-O-(2-O-[2-azidomethylbenzoyl]-3,4-di-O-benzyl-6-O-hexadecanoyl-α-D-mannopyranosyl)-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol

: 2-O-(2-O-[2-azidomethylbenzoyl]-3,4-di-O-benzyl-6-O-hexadecanoyl-α-D-mannopyranosyl)-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol

Guidance literature:: 1-O-allyl-2-O-(2-O-[2-azidomethylbenzoyl]-3,4-di-O-benzyl-6-O-hexadecanoyl-α-D-mannopyranosyl)-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-3,4,5-tri-O-benzyl-D-myo-inositol; With (1,5-cyclooctadiene)[bis(methyldiphenylphosphine)]iridium(I) hexafluorophosphate; In tetrahydrofuran; at 20 ℃; for 0.166667h; Inert atmosphere;

With hydrogen; In tetrahydrofuran; for 0.758333h; Inert atmosphere;

With acetyl chloride; In methanol; dichloromethane; at 20 ℃; for 1h;
DOI:10.1021/jm2008419