Technology Process of C23H25FN4O4S*ClH
There total 11 articles about C23H25FN4O4S*ClH which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C30H31FN4O4S;
With
trifluoroacetic acid;
at 20 ℃;
for 4h;
With
hydrogenchloride;
In
ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C
2.1: Lawessons reagent / tetrahydrofuran / 50 °C
2.2: 1 h / 20 °C
3.1: oxalyl dichloride / N,N-dimethyl-formamide / toluene / 2 h / 20 °C
3.2: 20 °C
4.1: trifluoroacetic acid / 0.33 h / 20 °C
4.2: 0.25 h / 20 °C
4.3: 0.33 h / 100 °C
5.1: trifluoroacetic acid / 4 h / 20 °C
With
Lawessons reagent; oxalyl dichloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid;
N,N-dimethyl-formamide;
In
tetrahydrofuran; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: lithium hexamethyldisilazane / tetrahydrofuran; ethylbenzene / 0.38 h / -70 °C
1.2: 0.42 h / -70 °C
1.3: 1 h / 20 °C
2.1: hydrogenchloride / ethyl acetate / 1 h / 20 °C
3.1: oxalyl dichloride / N,N-dimethyl-formamide / toluene / 2 h / 20 °C
3.2: 20 °C
4.1: trifluoroacetic acid / 0.33 h / 20 °C
4.2: 0.25 h / 20 °C
4.3: 0.33 h / 100 °C
5.1: trifluoroacetic acid / 4 h / 20 °C
With
hydrogenchloride; oxalyl dichloride; trifluoroacetic acid; lithium hexamethyldisilazane;
N,N-dimethyl-formamide;
In
tetrahydrofuran; ethylbenzene; ethyl acetate; toluene;
