5,5-difluoro-1,3,7,9-tetramethyl-10-(pyridin-4-yl)-5H-4λ⁴,5λ⁴-dipyrrolo [1,2-c:2′,1′-f][1-3]diazaborinine

Base Information

• Chemical Name: 5,5-difluoro-1,3,7,9-tetramethyl-10-(pyridin-4-yl)-5H-4λ⁴,5λ⁴-dipyrrolo [1,2-c:2′,1′-f][1-3]diazaborinine
• CAS No.: 1134484-25-5
• Molecular Formula: C₁₈H₁₈BF₂N₃
• Molecular Weight: 325.169
• Mol file: 1134484-25-5.mol

Synonyms:5,5-difluoro-1,3,7,9-tetramethyl-10-(pyridin-4-yl)-5H-4λ⁴,5λ⁴-dipyrrolo [1,2-c:2′,1′-f][1-3]diazaborinine

Chemical Property of 5,5-difluoro-1,3,7,9-tetramethyl-10-(pyridin-4-yl)-5H-4λ⁴,5λ⁴-dipyrrolo [1,2-c:2′,1′-f][1-3]diazaborinine

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5,5-difluoro-1,3,7,9-tetramethyl-10-(pyridin-4-yl)-5H-4λ⁴,5λ⁴-dipyrrolo [1,2-c:2′,1′-f][1-3]diazaborinine

There total 1 articles about 5,5-difluoro-1,3,7,9-tetramethyl-10-(pyridin-4-yl)-5H-4λ⁴,5λ⁴-dipyrrolo [1,2-c:2′,1′-f][1-3]diazaborinine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(4-azidobenzyl)-4-(5,5-difluoro-1,3,7,9-tetramethyl-5H-4λ4, 5λ4-dipyrrolo[1,2-c:2′,1′-f][1–3]diazaborinin-10-yl)pyridin-1-ium bromide → azaquinodimethane + 5,5-difluoro-1,3,7,9-tetramethyl-10-(pyridin-4-yl)-5H-4λ4,5λ4-dipyrrolo [1,2-c:2′,1′-f][1-3]diazaborinine (1134484-25-5)

Guidance literature:

In [D₃]acetonitrile; water-d2; for 2.5h;

DOI:10.1246/cl.150631

Reference yield: 93.0%

5,5-difluoro-1,3,7,9-tetramethyl-10-(pyridin-4-yl)-5H-4λ4,5λ4-dipyrrolo [1,2-c:2′,1′-f][1-3]diazaborinine (1134484-25-5) + C31H21F10IrN3P → C49H39BF6IrN6(1+)*F6P(1-)

Guidance literature:

In dichloromethane; at 20 ℃; for 18h; Glovebox;

DOI:10.1039/c9sc00696f

Reference yield: 75.0%

5,5-difluoro-1,3,7,9-tetramethyl-10-(pyridin-4-yl)-5H-4λ4,5λ4-dipyrrolo [1,2-c:2′,1′-f][1-3]diazaborinine (1134484-25-5) + 4-hydroxy-benzaldehyde (123-08-0,65581-83-1) → C32H26BF2N3O2

Guidance literature:

With piperidine; acetic acid; In toluene; for 10h; Reflux; Inert atmosphere;