trans-3-(3,4,5-trimethoxyphenyl)acrylic acid 3-[[2-(tert-butoxycarbonylmethylamino)ethyl]methylamino]propyl ester

Base Information

Chemical Name:trans-3-(3,4,5-trimethoxyphenyl)acrylic acid 3-[[2-(tert-butoxycarbonylmethylamino)ethyl]methylamino]propyl ester
CAS No.:870449-83-5
Molecular Formula:C₂₄H₃₈N₂O₇
Molecular Weight:466.575
Hs Code.:

Synonyms:trans-3-(3,4,5-trimethoxyphenyl)acrylic acid 3-[[2-(tert-butoxycarbonylmethylamino)ethyl]methylamino]propyl ester

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Chemical Property of trans-3-(3,4,5-trimethoxyphenyl)acrylic acid 3-[[2-(tert-butoxycarbonylmethylamino)ethyl]methylamino]propyl ester

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Technology Process of trans-3-(3,4,5-trimethoxyphenyl)acrylic acid 3-[[2-(tert-butoxycarbonylmethylamino)ethyl]methylamino]propyl ester

There total 3 articles about trans-3-(3,4,5-trimethoxyphenyl)acrylic acid 3-[[2-(tert-butoxycarbonylmethylamino)ethyl]methylamino]propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 870449-49-3
trans-3-(3,4,5-trimethoxyphenyl)acrylic acid 3-bromopropyl ester

: 112257-19-9
tert-butyl N-methyl-N-<2-(methylamino)ethyl>carbamate

: 870449-83-5
trans-3-(3,4,5-trimethoxyphenyl)acrylic acid 3-[[2-(tert-butoxycarbonylmethylamino)ethyl]methylamino]propyl ester

Guidance literature:: With potassium carbonate; In acetonitrile; at 60 ℃; for 6h;
DOI:10.1021/jm050542x

Reference yield:

: 20329-98-0,20329-99-1,90-50-6
(E)-3,4,5-trimethoxy-cinnamic acid

: 870449-83-5
trans-3-(3,4,5-trimethoxyphenyl)acrylic acid 3-[[2-(tert-butoxycarbonylmethylamino)ethyl]methylamino]propyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂ / benzene / 60 °C

2: CHCl₃ / 60 °C

3: 53 percent / K₂CO₃ / acetonitrile / 6 h / 60 °C

With thionyl chloride; potassium carbonate; In chloroform; acetonitrile; benzene;
DOI:10.1021/jm050542x

Reference yield:

: 10263-19-1,89652-61-9
(E)-3-(3,4,5-trimethoxyphenyl)acryloyl chloride

: 870449-83-5
trans-3-(3,4,5-trimethoxyphenyl)acrylic acid 3-[[2-(tert-butoxycarbonylmethylamino)ethyl]methylamino]propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: CHCl₃ / 60 °C

2: 53 percent / K₂CO₃ / acetonitrile / 6 h / 60 °C

With potassium carbonate; In chloroform; acetonitrile;
DOI:10.1021/jm050542x