(R)-N,N-bis(2-benzyloxy-3,5-di-tert-butylbenzyl)-1-(2-benzyloxy-3,5-di-tert-butylphenyl)ethylamine

Base Information

Chemical Name:(R)-N,N-bis(2-benzyloxy-3,5-di-tert-butylbenzyl)-1-(2-benzyloxy-3,5-di-tert-butylphenyl)ethylamine
CAS No.:925423-05-8
Molecular Formula:C₆₇H₈₉NO₃
Molecular Weight:956.449
Hs Code.:

Synonyms:(R)-N,N-bis(2-benzyloxy-3,5-di-tert-butylbenzyl)-1-(2-benzyloxy-3,5-di-tert-butylphenyl)ethylamine

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Chemical Property of (R)-N,N-bis(2-benzyloxy-3,5-di-tert-butylbenzyl)-1-(2-benzyloxy-3,5-di-tert-butylphenyl)ethylamine

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Technology Process of (R)-N,N-bis(2-benzyloxy-3,5-di-tert-butylbenzyl)-1-(2-benzyloxy-3,5-di-tert-butylphenyl)ethylamine

There total 7 articles about (R)-N,N-bis(2-benzyloxy-3,5-di-tert-butylbenzyl)-1-(2-benzyloxy-3,5-di-tert-butylphenyl)ethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 925423-04-7
2-(benzyloxy)-1-(bromomethyl)-3,5-di-tert-butylbenzene

: 925423-03-6
(R)-1-(2-benzyloxy-3,5-di-tert-butylphenyl)ethylamine

: 925423-05-8
(R)-N,N-bis(2-benzyloxy-3,5-di-tert-butylbenzyl)-1-(2-benzyloxy-3,5-di-tert-butylphenyl)ethylamine

Guidance literature:: With 4 A molecular sieve; potassium carbonate; sodium iodide; In N,N-dimethyl-formamide; for 48h;
DOI:10.1021/ol062655w

Reference yield:

: 71809-03-5
2-(benzyloxy)-3,5-di-tert-butylbenzaldehyde

: 925423-05-8
(R)-N,N-bis(2-benzyloxy-3,5-di-tert-butylbenzyl)-1-(2-benzyloxy-3,5-di-tert-butylphenyl)ethylamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: 95 percent / molecular sieves 4 Angstroem / ethanol / 20 h / 20 °C

2.1: 44 percent / tetrahydrofuran; diethyl ether / 16 h / -85 - 20 °C

3.1: lead(IV) acetate / CH₂Cl₂; methanol / 0.08 h / 0 °C

3.2: 66 percent / HCl / tetrahydrofuran; H₂O / 4 h / 80 °C

4.1: 64 percent / sodium iodide; potassium carbonate; molecular sieves 4 Angstroem / dimethylformamide / 48 h

With lead(IV) acetate; 4 A molecular sieve; potassium carbonate; sodium iodide; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol062655w

Reference yield:

: 37942-07-7
3,5-di-tert-butyl-2-hydroxybenzaldehyde

: 925423-05-8
(R)-N,N-bis(2-benzyloxy-3,5-di-tert-butylbenzyl)-1-(2-benzyloxy-3,5-di-tert-butylphenyl)ethylamine

Guidance literature:: Multi-step reaction with 5 steps

1.1: 99 percent / potassium carbonate / dimethylformamide / 20 h / 20 °C

2.1: 95 percent / molecular sieves 4 Angstroem / ethanol / 20 h / 20 °C

3.1: 44 percent / tetrahydrofuran; diethyl ether / 16 h / -85 - 20 °C

4.1: lead(IV) acetate / CH₂Cl₂; methanol / 0.08 h / 0 °C

4.2: 66 percent / HCl / tetrahydrofuran; H₂O / 4 h / 80 °C

5.1: 64 percent / sodium iodide; potassium carbonate; molecular sieves 4 Angstroem / dimethylformamide / 48 h

With lead(IV) acetate; 4 A molecular sieve; potassium carbonate; sodium iodide; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol062655w