methyl (1S,6R)-1,6-dihydroxycyclohex-2-enecarboxylate

Base Information

Chemical Name:methyl (1S,6R)-1,6-dihydroxycyclohex-2-enecarboxylate
CAS No.:1210906-76-5
Molecular Formula:C₈H₁₂O₄
Molecular Weight:172.181
Hs Code.:

Synonyms:methyl (1S,6R)-1,6-dihydroxycyclohex-2-enecarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (1S,6R)-1,6-dihydroxycyclohex-2-enecarboxylate

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Technology Process of methyl (1S,6R)-1,6-dihydroxycyclohex-2-enecarboxylate

There total 6 articles about methyl (1S,6R)-1,6-dihydroxycyclohex-2-enecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1210906-75-4
methyl 2,2-dimethyl-7,7a-dihydro-6H-benzo[d][1,3]dioxole-3a-carboxylate

: 1210906-76-5
methyl (1S,6R)-1,6-dihydroxycyclohex-2-enecarboxylate

Guidance literature:: With toluene-4-sulfonic acid; acetic acid; In tetrahydrofuran; water; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ol9029676

Reference yield: 40.0%

: 172877-72-4
(-)-(1S,6R)-methyl 1,6-dihydroxycyclohexa-2,4-dienecarboxylate

: 1210906-76-5
methyl (1S,6R)-1,6-dihydroxycyclohex-2-enecarboxylate

: 1310051-99-0
C₈H₁₂O₄

Guidance literature:: (-)-(1S,6R)-methyl 1,6-dihydroxycyclohexa-2,4-dienecarboxylate; With potassium diazodicarboxylate; In methanol; at 5 ℃; for 0.333333h; Inert atmosphere;

With acetic acid; In methanol; at 5 - 20 ℃; Inert atmosphere;
DOI:10.1055/s-0030-1259694

Reference yield:

: C₁₃H₂₀O₅S₂

: 1210906-76-5
methyl (1S,6R)-1,6-dihydroxycyclohex-2-enecarboxylate

Guidance literature:: C₁₃H₂₀O₅S₂; In diphenylether; at 230 ℃; for 0.5h; Inert atmosphere;

With toluene-4-sulfonic acid; acetic acid; In tetrahydrofuran; diphenylether; water; at 60 ℃; for 6h; Inert atmosphere;
DOI:10.1021/ol9029676