2-Iodo-1,3,4-trimethoxybenzene

Base Information

Chemical Name:2-Iodo-1,3,4-trimethoxybenzene
CAS No.:25245-42-5
Molecular Formula:C₉H₁₁IO₃
Molecular Weight:294.089
Hs Code.:
DSSTox Substance ID:DTXSID401305451

Synonyms:25245-42-5;2-iodo-1,3,4-trimethoxybenzene;SCHEMBL6720583;DTXSID401305451;Benzene, 2-iodo-1,3,4-trimethoxy-

Suppliers and Price of 2-Iodo-1,3,4-trimethoxybenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Iodo-1,3,4-trimethoxybenzene

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:293.97529
Heavy Atom Count:13
Complexity:154

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C(=C(C=C1)OC)I)OC

Technology Process of 2-Iodo-1,3,4-trimethoxybenzene

There total 2 articles about 2-Iodo-1,3,4-trimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.5%

: 135-77-3
1,2,4-trimethoxy-benzene

: 25245-42-5
iodo-1,2,4-trimethoxybenzene

Guidance literature:: 1,2,4-trimethoxy-benzene; With n-butyllithium; In diethyl ether; hexane; for 2h; Inert atmosphere; Reflux;

With iodine; In diethyl ether; hexane; at 20 ℃; for 1h; Inert atmosphere; Reflux;
DOI:10.1139/v11-008

Reference yield:

: 109-72-8,29786-93-4
n-butyllithium

: 135-77-3
1,2,4-trimethoxy-benzene

: 25245-42-5
iodo-1,2,4-trimethoxybenzene

Guidance literature:: With diethyl ether; Behandeln der Reaktionsloesung mit Jod;
DOI:10.1021/ja01234a002

Reference yield: 76.0%

: 25245-42-5
iodo-1,2,4-trimethoxybenzene

: (+)salvia sclarea tosylhydrazone

: C₂₃H₃₄O₄

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; at 110 ℃; for 10h; Inert atmosphere;