all-cis-4,4',6,6'-tetrakis(tert-butoxycarbonylamino)-6,6'-p-xylylidenebis(cyclohexane)-1,3,5-triol

Base Information

Chemical Name:all-cis-4,4',6,6'-tetrakis(tert-butoxycarbonylamino)-6,6'-p-xylylidenebis(cyclohexane)-1,3,5-triol
CAS No.:676154-41-9
Molecular Formula:C₄₀H₆₈N₆O₁₄
Molecular Weight:857.012
Hs Code.:

Synonyms:all-cis-4,4',6,6'-tetrakis(tert-butoxycarbonylamino)-6,6'-p-xylylidenebis(cyclohexane)-1,3,5-triol

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Chemical Property of all-cis-4,4',6,6'-tetrakis(tert-butoxycarbonylamino)-6,6'-p-xylylidenebis(cyclohexane)-1,3,5-triol

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Technology Process of all-cis-4,4',6,6'-tetrakis(tert-butoxycarbonylamino)-6,6'-p-xylylidenebis(cyclohexane)-1,3,5-triol

There total 1 articles about all-cis-4,4',6,6'-tetrakis(tert-butoxycarbonylamino)-6,6'-p-xylylidenebis(cyclohexane)-1,3,5-triol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 623-24-5
1,4-bis(bromomethyl)benzene

: 676154-38-4
all-cis-2-amino-4,6-bis(tert-butoxycarbonylamino)cyclohexane-1,3,5-triol

: 676154-41-9
all-cis-4,4',6,6'-tetrakis(tert-butoxycarbonylamino)-6,6'-p-xylylidenebis(cyclohexane)-1,3,5-triol

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 70 ℃; for 48h;
DOI:10.1002/ejoc.200300381

Reference yield: 89.0%

: 676154-41-9
all-cis-4,4',6,6'-tetrakis(tert-butoxycarbonylamino)-6,6'-p-xylylidenebis(cyclohexane)-1,3,5-triol

: C₂₀H₃₆N₆O₆*6HCl

Guidance literature:: all-cis-4,4',6,6'-tetrakis(tert-butoxycarbonylamino)-6,6'-p-xylylidenebis(cyclohexane)-1,3,5-triol; With trifluoroacetic acid; In dichloromethane; for 4h;

With DOVEX 50WX₂ (ion-exchange column, Cl^(1-) form); Further stages.;
DOI:10.1002/ejoc.200300381