4-(5-nitroindolin-1-yl)phenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

Base Information

Chemical Name:4-(5-nitroindolin-1-yl)phenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside
CAS No.:1312312-41-6
Molecular Formula:C₂₈H₃₀N₂O₁₂
Molecular Weight:586.552
Hs Code.:

Synonyms:4-(5-nitroindolin-1-yl)phenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

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Chemical Property of 4-(5-nitroindolin-1-yl)phenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

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Technology Process of 4-(5-nitroindolin-1-yl)phenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

There total 4 articles about 4-(5-nitroindolin-1-yl)phenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 32692-19-6
5-nitro-2,3-dihydro-1H-indole

: 287967-74-2
(2R,3R,4S,5S,6R)-2-(acetoxymethyl)-6-(4-iodophenoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

: 1312312-41-6
4-(5-nitroindolin-1-yl)phenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

Guidance literature:: With caesium carbonate; XPhos; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In toluene; at 80 ℃; for 140h; Inert atmosphere;

Reference yield:

: 121238-27-5
2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl trichloroimidate

: 1312312-41-6
4-(5-nitroindolin-1-yl)phenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: trimethylsilyl trifluoromethanesulfonate / toluene / 2.5 h / 20 °C / Inert atmosphere

2: caesium carbonate; XPhos / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 140 h / 80 °C / Inert atmosphere

With trimethylsilyl trifluoromethanesulfonate; caesium carbonate; XPhos; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In toluene;

Reference yield:

: 22860-22-6
2,3,4,6-tetra-O-acetyl-α-D-mannopyranose

: 1312312-41-6
4-(5-nitroindolin-1-yl)phenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate / dichloromethane / 3.5 h / 20 °C / Inert atmosphere

2: trimethylsilyl trifluoromethanesulfonate / toluene / 2.5 h / 20 °C / Inert atmosphere

3: caesium carbonate; XPhos / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 140 h / 80 °C / Inert atmosphere

With trimethylsilyl trifluoromethanesulfonate; caesium carbonate; XPhos; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In dichloromethane; toluene;