(Z)-3-ethylidenecyclohexanol

Base Information

Chemical Name:(Z)-3-ethylidenecyclohexanol
CAS No.:110774-45-3
Molecular Formula:C₈H₁₄O
Molecular Weight:126.199
Hs Code.:

Synonyms:(Z)-3-ethylidenecyclohexanol

Suppliers and Price of (Z)-3-ethylidenecyclohexanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-3-ethylidenecyclohexanol

Chemical Property:

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Technology Process of (Z)-3-ethylidenecyclohexanol

There total 5 articles about (Z)-3-ethylidenecyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110774-36-2
5-ethyl-5-hexanal

: 110774-44-2
(E)-3-ethylidenecyclohexanol

: 110774-45-3
(Z)-3-ethylidenecyclohexanol

Guidance literature:: With dimethylaluminum chloride; In hexane; dichloromethane; at -78 ℃; for 0.5h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/jo00233a021

Reference yield:

: 71097-17-1
5-ethyl-5-hexen-1-ol

: 110774-45-3
(Z)-3-ethylidenecyclohexanol

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / PDC / CH₂Cl₂ / Ambient temperature

2: Me₂AlCl / CH₂Cl₂ / -78 °C

With dipyridinium dichromate; dimethylaluminum chloride; In dichloromethane;
DOI:10.1016/S0040-4020(01)89682-4

Reference yield:

: 67448-61-7
6-(1-ethoxy-ethoxy)-hex-1-yne

: 110774-45-3
(Z)-3-ethylidenecyclohexanol

Guidance literature:: Multi-step reaction with 3 steps

1: 54 percent / cuprous bromide-dimethyl sulfide complex / diethyl ether; various solvent(s) / 2 h / -45 °C

2: 82 percent / CrO₃, pyridine / CH₂Cl₂ / 25 °C

3: Me₂AlCl / CH₂Cl₂; hexane / 0.5 h / -78 °C

With pyridine; chromium(VI) oxide; copper(I) bromide dimethylsulfide complex; dimethylaluminum chloride; In diethyl ether; hexane; dichloromethane;
DOI:10.1021/jo00233a021