(6-(4-methoxyphenyl)-12-phenyl-6H-naphtho[2,3-c]chromen-7-yl)diphenylphosphine oxide

Base Information

Chemical Name:(6-(4-methoxyphenyl)-12-phenyl-6H-naphtho[2,3-c]chromen-7-yl)diphenylphosphine oxide
CAS No.:1609662-53-4
Molecular Formula:C₄₂H₃₁O₃P
Molecular Weight:614.68
Hs Code.:

Synonyms:(6-(4-methoxyphenyl)-12-phenyl-6H-naphtho[2,3-c]chromen-7-yl)diphenylphosphine oxide

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Chemical Property of (6-(4-methoxyphenyl)-12-phenyl-6H-naphtho[2,3-c]chromen-7-yl)diphenylphosphine oxide

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Technology Process of (6-(4-methoxyphenyl)-12-phenyl-6H-naphtho[2,3-c]chromen-7-yl)diphenylphosphine oxide

There total 3 articles about (6-(4-methoxyphenyl)-12-phenyl-6H-naphtho[2,3-c]chromen-7-yl)diphenylphosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 92151-73-0
2-phenylethynylphenol

: 1609661-59-7
(1-(2-bromophenyl)-3-(4-methoxyphenyl)propa-1,2-dien-1-yl)diphenylphosphine oxide

: 1609662-53-4
(6-(4-methoxyphenyl)-12-phenyl-6H-naphtho[2,3-c]chromen-7-yl)diphenylphosphine oxide

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; tricyclohexylphosphine; In 1,4-dioxane; at 100 ℃; regioselective reaction;
DOI:10.1039/c4cc00374h

Reference yield:

: 19115-30-1
1-(4-methoxyphenyl)-2-propyn-1-ol

: 1609662-53-4
(6-(4-methoxyphenyl)-12-phenyl-6H-naphtho[2,3-c]chromen-7-yl)diphenylphosphine oxide

Guidance literature:: Multi-step reaction with 3 steps

1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / 20 °C / Inert atmosphere

2: triethylamine / tetrahydrofuran / 4 h / -78 - 20 °C

3: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tricyclohexylphosphine; potassium carbonate / 1,4-dioxane / 100 °C

With bis-triphenylphosphine-palladium(II) chloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; potassium carbonate; triethylamine; tricyclohexylphosphine; In tetrahydrofuran; 1,4-dioxane; 1: |Sonogashira Cross-Coupling;
DOI:10.1039/c4cc00374h

Reference yield:

: 1609661-88-2
3-(2-bromophenyl)-1-(4-methoxyphenyl)prop-2-yn-1-ol

: 1609662-53-4
(6-(4-methoxyphenyl)-12-phenyl-6H-naphtho[2,3-c]chromen-7-yl)diphenylphosphine oxide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 4 h / -78 - 20 °C

2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tricyclohexylphosphine; potassium carbonate / 1,4-dioxane / 100 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; triethylamine; tricyclohexylphosphine; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1039/c4cc00374h