bis<4-phenyl> disulfide

Base Information

• Chemical Name: bis<4-phenyl> disulfide
• CAS No.: 131042-38-1
• Molecular Formula: C₂₀H₂₈N₂O₂S₂
• Molecular Weight: 392.587

Synonyms:bis<4-phenyl> disulfide

Chemical Property of bis<4-phenyl> disulfide

Chemical Property:

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Technology Process of bis<4-phenyl> disulfide

There total 7 articles about bis<4-phenyl> disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

4-benzenethiol (131042-37-0) → methyl 3-<<4-phenyl>thio>propanoate (131042-39-2) + bis<4-phenyl> disulfide (131042-38-1)

Guidance literature:

With Methyl 3-bromopropionate; potassium carbonate; In methanol; for 0.5h; Heating;

DOI:10.1021/jm00105a038

Reference yield: 27.0%

S-(benzyloxycarbonyl)-4-benzenethiol (131042-36-9) → 4-benzenethiol (131042-37-0) + bis<4-phenyl> disulfide (131042-38-1)

Guidance literature:

With sodium hydroxide; In ethanol; for 20h; Ambient temperature;

DOI:10.1021/jm00105a038

Reference yield: 14.0%

Methyl 3-bromopropionate (3395-91-3) + 4-benzenethiol (131042-37-0) → methyl 3-<<4-phenyl>thio>propanoate (131042-39-2) + bis<4-phenyl> disulfide (131042-38-1)

Guidance literature:

With potassium carbonate; In methanol; for 0.5h; Heating;

DOI:10.1021/jm00105a038

upstream raw materials:

Methyl 3-bromopropionate

4-benzenethiol

S-(benzyloxycarbonyl)-4-benzenethiol

S-<(benzyloxy)carbonyl>-4-aminobenzenethiol

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