2,4-di-O-acetyl-3,6-di-O-(4-methylbenzoyl)-α-D-mannopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-α-D-glucopyranosyl dibenzyl phosphate

Base Information

Chemical Name:2,4-di-O-acetyl-3,6-di-O-(4-methylbenzoyl)-α-D-mannopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-α-D-glucopyranosyl dibenzyl phosphate
CAS No.:663603-96-1
Molecular Formula:C₆₄H₇₅N₂O₂₇P
Molecular Weight:1335.27
Hs Code.:

2,4-di-O-acetyl-3,6-di-O-(4-methylbenzoyl)-α-D-mannopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-α-D-glucopyranosyl dibenzyl phosphate

Synonyms:2,4-di-O-acetyl-3,6-di-O-(4-methylbenzoyl)-α-D-mannopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-α-D-glucopyranosyl dibenzyl phosphate

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Chemical Property of 2,4-di-O-acetyl-3,6-di-O-(4-methylbenzoyl)-α-D-mannopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-α-D-glucopyranosyl dibenzyl phosphate

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Technology Process of 2,4-di-O-acetyl-3,6-di-O-(4-methylbenzoyl)-α-D-mannopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-α-D-glucopyranosyl dibenzyl phosphate

There total 2 articles about 2,4-di-O-acetyl-3,6-di-O-(4-methylbenzoyl)-α-D-mannopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-α-D-glucopyranosyl dibenzyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 663603-95-0
2,4-di-O-acetyl-3,6-di-O-(4-methylbenzoyl)-α-D-mannopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranose

: 990-91-0
dibenzyl [[bis(benzyloxy)phosphoryl]oxy]phosphonate

: 663603-96-1
2,4-di-O-acetyl-3,6-di-O-(4-methylbenzoyl)-α-D-mannopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-α-D-glucopyranosyl dibenzyl phosphate

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1.5h;
DOI:10.1271/bbb.67.1761

Reference yield:

: 2,4-di-O-acetyl-3,6-di-O-(4-methylbenzoyl)-α-D-mannopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->4)-2-acetamido-1,3,6-tri-O-acetyl-2-deoxy-α/β-D-glucopyranose

: 663603-96-1
2,4-di-O-acetyl-3,6-di-O-(4-methylbenzoyl)-α-D-mannopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->4)-2-acetamido-3,6-di-O-acetyl-2-deoxy-α-D-glucopyranosyl dibenzyl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / hydrazine acetate / dimethylformamide / 0.5 h / 20 °C

2: 85 percent / n-BuLi / tetrahydrofuran; hexane / 1.5 h / -78 °C

With n-butyllithium; hydrazinium monoacetate; In tetrahydrofuran; hexane; N,N-dimethyl-formamide;
DOI:10.1271/bbb.67.1761