2,12-bis(9-anthracenyl)-7-(4-(dimethylamino)phenyl)-5,6,8,9-tetrahydro-1,13-diazadibenzxanthene

Base Information

Chemical Name:2,12-bis(9-anthracenyl)-7-(4-(dimethylamino)phenyl)-5,6,8,9-tetrahydro-1,13-diazadibenzxanthene
CAS No.:123030-25-1
Molecular Formula:C₅₅H₄₁N₃O
Molecular Weight:759.95
Hs Code.:

2,12-bis(9-anthracenyl)-7-(4-(dimethylamino)phenyl)-5,6,8,9-tetrahydro-1,13-diazadibenz<a,j>xanthene

Synonyms:2,12-bis(9-anthracenyl)-7-(4-(dimethylamino)phenyl)-5,6,8,9-tetrahydro-1,13-diazadibenzxanthene

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Chemical Property of 2,12-bis(9-anthracenyl)-7-(4-(dimethylamino)phenyl)-5,6,8,9-tetrahydro-1,13-diazadibenzxanthene

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Technology Process of 2,12-bis(9-anthracenyl)-7-(4-(dimethylamino)phenyl)-5,6,8,9-tetrahydro-1,13-diazadibenzxanthene

There total 4 articles about 2,12-bis(9-anthracenyl)-7-(4-(dimethylamino)phenyl)-5,6,8,9-tetrahydro-1,13-diazadibenzxanthene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 784-04-3
9-acetylanthracene

: 123030-25-1
2,12-bis(9-anthracenyl)-7-(4-(dimethylamino)phenyl)-5,6,8,9-tetrahydro-1,13-diazadibenzxanthene

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) Me₂NH*HCl / 1.) EtOH, reflux; 2.) 160 deg C

2: NH₄OAc / acetic acid / Heating

4: 1.) KOH; 2.) BF₃*OEt₂ / 1.) MeOH

With potassium hydroxide; boron trifluoride diethyl etherate; ammonium acetate; N,N-dimethylammonium chloride; In acetic acid;
DOI:10.1021/ja00202a077

Reference yield:

: 123030-22-8
1-(9-anthracenyl)-3-(2-oxo-1-cyclohexyl)-1-propanone

: 123030-25-1
2,12-bis(9-anthracenyl)-7-(4-(dimethylamino)phenyl)-5,6,8,9-tetrahydro-1,13-diazadibenzxanthene

Guidance literature:: Multi-step reaction with 3 steps

1: NH₄OAc / acetic acid / Heating

3: 1.) KOH; 2.) BF₃*OEt₂ / 1.) MeOH

With potassium hydroxide; boron trifluoride diethyl etherate; ammonium acetate; In acetic acid;
DOI:10.1021/ja00202a077

Reference yield:

: 123030-23-9
2-(9-anthracenyl)-5,6,7,8-tetrahydroquinoline

: 123030-25-1
2,12-bis(9-anthracenyl)-7-(4-(dimethylamino)phenyl)-5,6,8,9-tetrahydro-1,13-diazadibenzxanthene

Guidance literature:: Multi-step reaction with 2 steps

2: 1.) KOH; 2.) BF₃*OEt₂ / 1.) MeOH

With potassium hydroxide; boron trifluoride diethyl etherate;
DOI:10.1021/ja00202a077