(R)-methyl 2,3-dihydro-5-oxo-12-phenylbenzo[g]thiazolo[3,2-b]isoquinoline-3-carboxylate

Base Information

Chemical Name:(R)-methyl 2,3-dihydro-5-oxo-12-phenylbenzo[g]thiazolo[3,2-b]isoquinoline-3-carboxylate
CAS No.:1257337-50-0
Molecular Formula:C₂₃H₁₇NO₃S
Molecular Weight:387.459
Hs Code.:

Synonyms:(R)-methyl 2,3-dihydro-5-oxo-12-phenylbenzo[g]thiazolo[3,2-b]isoquinoline-3-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-methyl 2,3-dihydro-5-oxo-12-phenylbenzo[g]thiazolo[3,2-b]isoquinoline-3-carboxylate

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Technology Process of (R)-methyl 2,3-dihydro-5-oxo-12-phenylbenzo[g]thiazolo[3,2-b]isoquinoline-3-carboxylate

There total 1 articles about (R)-methyl 2,3-dihydro-5-oxo-12-phenylbenzo[g]thiazolo[3,2-b]isoquinoline-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1257337-62-4
(R)-methyl 7-benzyl-6-formyl-2,3-dihydro-5-oxo-8-phenylthiazolo[3,2-a]pyridine-3-carboxylate

: 1257337-50-0
(R)-methyl 2,3-dihydro-5-oxo-12-phenylbenzo[g]thiazolo[3,2-b]isoquinoline-3-carboxylate

Guidance literature:: With titanium tetrachloride; In dichloromethane; at 100 ℃; for 0.833333h; Microwave irradiation;
DOI:10.1002/ejoc.201000796

Reference yield: 93.0%

: 1257337-50-0
(R)-methyl 2,3-dihydro-5-oxo-12-phenylbenzo[g]thiazolo[3,2-b]isoquinoline-3-carboxylate

: 1263361-29-0
C₂₂H₁₅NO₃S

Guidance literature:: With water; lithium hydroxide; In tetrahydrofuran; methanol; at 20 ℃; Inert atmosphere;
DOI:10.1021/la104051z

Reference yield:

: 1257337-50-0
(R)-methyl 2,3-dihydro-5-oxo-12-phenylbenzo[g]thiazolo[3,2-b]isoquinoline-3-carboxylate

: 1263361-27-8
1,2-di(2,3-dihydro-12-phenyl-benzo[g]thiazolo[3,2-b]isoquinoline-5-one-3-carboxylate)ethane

: 1,2-di(2,3-dihydro-12-phenyl-benzo[g]thiazolo[3,2-b]isoquinoline-5-one-3-carboxylate)ethane

Guidance literature:: Multi-step reaction with 2 steps

1: water; lithium hydroxide / tetrahydrofuran; methanol / 20 °C / Inert atmosphere

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 20 °C / Inert atmosphere

With dmap; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide; In tetrahydrofuran; methanol;
DOI:10.1021/la104051z