C₁₄H₁₁F₃O₃

Base Information

• Chemical Name: C₁₄H₁₁F₃O₃
• CAS No.: 1457998-56-9
• Molecular Formula: C₁₄H₁₁F₃O₃
• Molecular Weight: 284.235

Synonyms:C₁₄H₁₁F₃O₃

Chemical Property of C₁₄H₁₁F₃O₃

Chemical Property:

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Technology Process of C₁₄H₁₁F₃O₃

There total 3 articles about C₁₄H₁₁F₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C14H11F3O2 (1457998-40-1) → C14H11F3O3 (1457998-53-6) + C14H11F3O3 (1457998-56-9)

Guidance literature:

With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 24h; Overall yield = 65 %; Overall yield = 111 mg; Molecular sieve;

DOI:10.1016/j.jfluchem.2013.07.017

Reference yield:

C22H31F3O3Si → C14H11F3O3 (1457998-53-6) + C14H11F3O3 (1457998-56-9)

Guidance literature:

Multi-step reaction with 3 steps

1: triethylamine tris(hydrogen fluoride) / acetonitrile / 12 h / 30 °C

2: toluene-4-sulfonic acid / benzene / 24 h / 30 °C

3: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 20 °C / Molecular sieve

With sodium hydrogencarbonate; toluene-4-sulfonic acid; triethylamine tris(hydrogen fluoride); 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetonitrile; benzene;

DOI:10.1016/j.jfluchem.2013.07.017

Reference yield:

C16H17F3O3 → C14H11F3O3 (1457998-53-6) + C14H11F3O3 (1457998-56-9)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / benzene / 24 h / 30 °C

2: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 20 °C / Molecular sieve

With sodium hydrogencarbonate; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; benzene;

DOI:10.1016/j.jfluchem.2013.07.017

upstream raw materials:

C₁₄H₁₁F₃O₂

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