phenyl 4-O-acetyl-2,6-diazido-2,6-dideoxy-3-O-benzyl-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:phenyl 4-O-acetyl-2,6-diazido-2,6-dideoxy-3-O-benzyl-1-thio-β-D-glucopyranoside
CAS No.:1245566-86-2
Molecular Formula:C₂₁H₂₂N₆O₄S
Molecular Weight:454.509
Hs Code.:

Synonyms:phenyl 4-O-acetyl-2,6-diazido-2,6-dideoxy-3-O-benzyl-1-thio-β-D-glucopyranoside

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Chemical Property of phenyl 4-O-acetyl-2,6-diazido-2,6-dideoxy-3-O-benzyl-1-thio-β-D-glucopyranoside

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Technology Process of phenyl 4-O-acetyl-2,6-diazido-2,6-dideoxy-3-O-benzyl-1-thio-β-D-glucopyranoside

There total 3 articles about phenyl 4-O-acetyl-2,6-diazido-2,6-dideoxy-3-O-benzyl-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1245566-85-1
C₁₉H₂₀N₆O₃S

: 108-24-7
acetic anhydride

: 1245566-86-2
phenyl 4-O-acetyl-2,6-diazido-2,6-dideoxy-3-O-benzyl-1-thio-β-D-glucopyranoside

Guidance literature:: With pyridine; at 20 ℃; for 28h; Inert atmosphere;

Reference yield:

: 666753-83-9
phenyl 2-azido-3-O-benzyl-2-deoxy-1-thio-β-D-glucopyranoside

: 1245566-86-2
phenyl 4-O-acetyl-2,6-diazido-2,6-dideoxy-3-O-benzyl-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / -15 °C / Inert atmosphere

2: sodium azide / N,N-dimethyl-formamide / 12 h / 80 °C / Inert atmosphere

3: pyridine / 28 h / 20 °C / Inert atmosphere

With pyridine; sodium azide; In N,N-dimethyl-formamide;
DOI:10.1021/jo200951p

Reference yield:

: 1245566-82-8
C₂₀H₂₃N₃O₆S₂

: 1245566-86-2
phenyl 4-O-acetyl-2,6-diazido-2,6-dideoxy-3-O-benzyl-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / N,N-dimethyl-formamide / 12 h / 80 °C / Inert atmosphere

2: pyridine / 28 h / 20 °C / Inert atmosphere

With pyridine; sodium azide; In N,N-dimethyl-formamide;
DOI:10.1021/jo200951p