1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-3-tert-butoxycarbonylmethylthymine

Base Information

Chemical Name:1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-3-tert-butoxycarbonylmethylthymine
CAS No.:799261-97-5
Molecular Formula:C₃₇H₃₆N₂O₁₁
Molecular Weight:684.7
Hs Code.:

Synonyms:1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-3-tert-butoxycarbonylmethylthymine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-3-tert-butoxycarbonylmethylthymine

Chemical Property:

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Technology Process of 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-3-tert-butoxycarbonylmethylthymine

There total 3 articles about 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-3-tert-butoxycarbonylmethylthymine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 3180-76-5
2',3',5'-tri-O-benzoyluridine

: 5292-43-3
bromoacetic acid tert-butyl ester

: 799261-97-5
1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-3-tert-butoxycarbonylmethylthymine

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1081/NCN-200067423

Reference yield:

: 65-71-4,28806-14-6,691841-57-3
thymin

: 799261-97-5
1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-3-tert-butoxycarbonylmethylthymine

Guidance literature:: Multi-step reaction with 3 steps

1: HMDS / 1,2-dichloro-ethane / 3 h / 80 °C

2: 91 percent / SnCl₄ / 1,2-dichloro-ethane / 2 h / 20 °C

3: 99 percent / potassium carbonate / dimethylformamide / 2 h / 20 °C

With tin(IV) chloride; potassium carbonate; 1,1,1,3,3,3-hexamethyl-disilazane; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1081/NCN-200067423

Reference yield:

: 7288-28-0
2,4-bis(trimethylsiloxy)-5-methylpyrimidine

: 799261-97-5
1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-3-tert-butoxycarbonylmethylthymine

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / SnCl₄ / 1,2-dichloro-ethane / 2 h / 20 °C

2: 99 percent / potassium carbonate / dimethylformamide / 2 h / 20 °C

With tin(IV) chloride; potassium carbonate; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1081/NCN-200067423