2,3-dimethoxycinnamoyl chloride

Base Information

• Chemical Name: 2,3-dimethoxycinnamoyl chloride
• CAS No.: 39157-03-4
• Molecular Formula: C₁₁H₁₁ClO₃
• Molecular Weight: 226.66

Synonyms:2,3-dimethoxycinnamoyl chloride

Chemical Property of 2,3-dimethoxycinnamoyl chloride

Chemical Property:

Purity/Quality:

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Technology Process of 2,3-dimethoxycinnamoyl chloride

There total 2 articles about 2,3-dimethoxycinnamoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3-dimethoxycinnamic acid (7461-60-1) → 2,3-dimethoxycinnamoyl chloride (39157-03-4)

Guidance literature:

With oxalyl dichloride; In dichloromethane; at 25 ℃;

DOI:10.3390/molecules14104166

Reference yield:

→ 2,3-dimethoxycinnamoyl chloride (39157-03-4)

Guidance literature:

2,3-Dimethoxy-zimtsaeure, SOCl2, Kochen, 45 min;

DOI:10.1021/jo01065a609

Reference yield: 83.0%

3-aminopiperidin-2-one (1892-22-4,4077-38-7,34294-79-6,88763-76-2) + 2,3-dimethoxycinnamoyl chloride (39157-03-4) → (E)-3-(2,3-Dimethoxy-phenyl)-N-(2-oxo-piperidin-3-yl)-acrylamide

Guidance literature:

With triethylamine; In tetrahydrofuran; for 2h; Ambient temperature;

DOI:10.1002/jhet.5570310432

upstream raw materials:

2,3-dimethoxycinnamic acid

Downstream raw materials:

2-(2,3-dimethoxystyryl)-4,5,6,7-tetrahydrothiazolo[5,4-b]pyridine

(E)-3-(2,3-dimethoxyphenyl)-N-[4-methyl-3-(4-pyridin-3-ylpyrimidin-2-ylamino)phenyl]acrylamide

N-(4-hydroxyphenyl)-2,3-dimethoxycinnamoylamide

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