(S)-(2-carboxy-4-oxoazetidine-1-carboxamido)phenylmethanaminium 2,2,2-trifluoroacetate

Base Information

Chemical Name:(S)-(2-carboxy-4-oxoazetidine-1-carboxamido)phenylmethanaminium 2,2,2-trifluoroacetate
CAS No.:1620568-08-2
Molecular Formula:C₂HF₃O₂*C₁₂H₁₃N₃O₄
Molecular Weight:377.277
Hs Code.:

Synonyms:(S)-(2-carboxy-4-oxoazetidine-1-carboxamido)phenylmethanaminium 2,2,2-trifluoroacetate

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Chemical Property of (S)-(2-carboxy-4-oxoazetidine-1-carboxamido)phenylmethanaminium 2,2,2-trifluoroacetate

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Technology Process of (S)-(2-carboxy-4-oxoazetidine-1-carboxamido)phenylmethanaminium 2,2,2-trifluoroacetate

There total 4 articles about (S)-(2-carboxy-4-oxoazetidine-1-carboxamido)phenylmethanaminium 2,2,2-trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1620568-17-3
C₁₇H₂₁N₃O₆

: 76-05-1
trifluoroacetic acid

: 1620568-08-2
(S)-(2-carboxy-4-oxoazetidine-1-carboxamido)phenylmethanaminium 2,2,2-trifluoroacetate

Guidance literature:: In dichloromethane; at 0 - 20 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.ejmech.2014.06.041

Reference yield:

: 178972-26-4
tert-butyl 4-isocyanatobenzylcarbamate

: 1620568-08-2
(S)-(2-carboxy-4-oxoazetidine-1-carboxamido)phenylmethanaminium 2,2,2-trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: 0.5 h / -78 °C / Inert atmosphere

2.1: palladium 10% on activated carbon; hydrogen / methanol; tetrahydrofuran / 2 h / 20 °C / 760.05 Torr

3.1: dichloromethane / 24 h / 0 - 20 °C / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; sodium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.ejmech.2014.06.041

Reference yield:

: 1620568-16-2
C₂₄H₂₇N₃O₆

: 1620568-08-2
(S)-(2-carboxy-4-oxoazetidine-1-carboxamido)phenylmethanaminium 2,2,2-trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / methanol; tetrahydrofuran / 2 h / 20 °C / 760.05 Torr

2: dichloromethane / 24 h / 0 - 20 °C / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.ejmech.2014.06.041