12c-methanesulfinyl-p-tolyl-4,8,12-tripropyl-12,12c-dihydro-4H,8H-4,8,12-triaza-dibenzo[cd,mn]pyrene

Base Information

• Chemical Name: 12c-methanesulfinyl-p-tolyl-4,8,12-tripropyl-12,12c-dihydro-4H,8H-4,8,12-triaza-dibenzo[cd,mn]pyrene
• CAS No.: 906377-54-6
• Molecular Formula: C₃₆H₃₉N₃OS
• Molecular Weight: 561.791

Synonyms:12c-methanesulfinyl-p-tolyl-4,8,12-tripropyl-12,12c-dihydro-4H,8H-4,8,12-triaza-dibenzo[cd,mn]pyrene

Chemical Property of 12c-methanesulfinyl-p-tolyl-4,8,12-tripropyl-12,12c-dihydro-4H,8H-4,8,12-triaza-dibenzo[cd,mn]pyrene

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Technology Process of 12c-methanesulfinyl-p-tolyl-4,8,12-tripropyl-12,12c-dihydro-4H,8H-4,8,12-triaza-dibenzo[cd,mn]pyrene

There total 1 articles about 12c-methanesulfinyl-p-tolyl-4,8,12-tripropyl-12,12c-dihydro-4H,8H-4,8,12-triaza-dibenzo[cd,mn]pyrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

Methyl p-tolyl sulfoxide (934-72-5) + 4,8,12-tri-n-propyl-4,8,12-triaza-triangulenium tetrafluoroborate → 12c-methanesulfinyl-p-tolyl-4,8,12-tripropyl-12,12c-dihydro-4H,8H-4,8,12-triaza-dibenzo[cd,mn]pyrene (906377-54-6)

Guidance literature:

Methyl p-tolyl sulfoxide; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at 0 ℃; for 0.5h;

4,8,12-tri-n-propyl-4,8,12-triaza-triangulenium tetrafluoroborate; In tetrahydrofuran; hexane; at 0 - 20 ℃; for 14h; Further stages.;

DOI:10.1039/b605187a

Reference yield: 98.0%

12c-methanesulfinyl-p-tolyl-4,8,12-tripropyl-12,12c-dihydro-4H,8H-4,8,12-triaza-dibenzo[cd,mn]pyrene (906377-54-6) + trifluoroacetic anhydride (407-25-0) → C2F3O2(1-)*C28H30N3(1+) (906377-59-1) + p-tolylthiomethyl 2,2,2-trifluoroacetate (103603-56-1)

Guidance literature:

In dichloromethane; at 20 ℃; for 0.333333h;

DOI:10.1039/b605187a

upstream raw materials:

Methyl p-tolyl sulfoxide

Downstream raw materials:

C₂F₃O₂^(1-)*C₂₈H₃₀N₃⁽¹⁺⁾

p-tolylthiomethyl 2,2,2-trifluoroacetate

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