Technology Process of C36H55ClN4O6
There total 5 articles about C36H55ClN4O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine / dichloromethane / 24 h / 20 °C
2: palladium hydroxide on carbon / ethanol; cyclohexane / 24 h / Heating / reflux
3: N-ethyl-N,N-diisopropylamine; potassium iodide / DMF (N,N-dimethyl-formamide) / 25 h / 40 - 80 °C
With
pyridine; N-ethyl-N,N-diisopropylamine; potassium iodide;
palladium hydroxide on carbon;
In
DMF (N,N-dimethyl-formamide); ethanol; dichloromethane; cyclohexane;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: palladium hydroxide on carbon / ethanol; cyclohexane / 24 h / Heating / reflux
2: N-ethyl-N,N-diisopropylamine; potassium iodide / DMF (N,N-dimethyl-formamide) / 25 h / 40 - 80 °C
With
N-ethyl-N,N-diisopropylamine; potassium iodide;
palladium hydroxide on carbon;
In
DMF (N,N-dimethyl-formamide); ethanol; cyclohexane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 °C
2: pyridine / dichloromethane / 24 h / 20 °C
3: palladium hydroxide on carbon / ethanol; cyclohexane / 24 h / Heating / reflux
4: N-ethyl-N,N-diisopropylamine; potassium iodide / DMF (N,N-dimethyl-formamide) / 25 h / 40 - 80 °C
With
pyridine; lithium aluminium tetrahydride; N-ethyl-N,N-diisopropylamine; potassium iodide;
palladium hydroxide on carbon;
In
tetrahydrofuran; DMF (N,N-dimethyl-formamide); ethanol; dichloromethane; cyclohexane;