1-Amino-7-[3-(3,4-dimethoxyphenethylamino)-2-hydroxypropyl]-8-oxoguanosine

Base Information

• Chemical Name: 1-Amino-7-[3-(3,4-dimethoxyphenethylamino)-2-hydroxypropyl]-8-oxoguanosine
• CAS No.: 1053627-83-0
• Molecular Formula: C₂₃H₃₃N₇O₉
• Molecular Weight: 551.557

Synonyms:1-Amino-7-[3-(3,4-dimethoxyphenethylamino)-2-hydroxypropyl]-8-oxoguanosine

Chemical Property of 1-Amino-7-[3-(3,4-dimethoxyphenethylamino)-2-hydroxypropyl]-8-oxoguanosine

Chemical Property:

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Technology Process of 1-Amino-7-[3-(3,4-dimethoxyphenethylamino)-2-hydroxypropyl]-8-oxoguanosine

There total 3 articles about 1-Amino-7-[3-(3,4-dimethoxyphenethylamino)-2-hydroxypropyl]-8-oxoguanosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

→ 7-[3-(3,4-dimethyoxyphenethylamino)-2-hydroxy]propyl-8-oxoguanosine monohydrochloride monohydrate + 1-Amino-7-[3-(3,4-dimethoxyphenethylamino)-2-hydroxypropyl]-8-oxoguanosine (1053627-83-0)

Guidance literature:

Reference yield:

1-amino-8-hydroxyguanosine (19029-70-0) → 1-Amino-7-[3-(3,4-dimethoxyphenethylamino)-2-hydroxypropyl]-8-oxoguanosine (1053627-83-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, RT, 5 min, 2.) DMF, overnight

2: dimethylformamide / 4 h / 80 °C

With sodium hydride; In N,N-dimethyl-formamide;

DOI:10.1021/jm00047a014

Reference yield:

2-(3,4-dimethoxyphenyl)-ethylamine (120-20-7) + 1,2-diamino-7-(2,3-epoxypropyl)-9-β-D-ribofuranosylpurine-6,8(1H)-dione (126092-33-9) → 1-Amino-7-[3-(3,4-dimethoxyphenethylamino)-2-hydroxypropyl]-8-oxoguanosine (1053627-83-0)

Guidance literature:

In N,N-dimethyl-formamide; at 80 ℃; for 4h;

DOI:10.1021/jm00047a014

upstream raw materials:

2-(3,4-dimethoxyphenyl)-ethylamine

1,2-diamino-7-(2,3-epoxypropyl)-9-β-D-ribofuranosylpurine-6,8(1H)-dione

1-amino-8-hydroxyguanosine

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