Naphthalene-1-carboxylic acid benzyl-((R)-2-hydroxy-1-phenyl-ethyl)-amide

Base Information

Chemical Name:Naphthalene-1-carboxylic acid benzyl-((R)-2-hydroxy-1-phenyl-ethyl)-amide
CAS No.:349663-29-2
Molecular Formula:C₂₆H₂₃NO₂
Molecular Weight:381.474
Hs Code.:

Synonyms:Naphthalene-1-carboxylic acid benzyl-((R)-2-hydroxy-1-phenyl-ethyl)-amide

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Chemical Property of Naphthalene-1-carboxylic acid benzyl-((R)-2-hydroxy-1-phenyl-ethyl)-amide

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Technology Process of Naphthalene-1-carboxylic acid benzyl-((R)-2-hydroxy-1-phenyl-ethyl)-amide

There total 4 articles about Naphthalene-1-carboxylic acid benzyl-((R)-2-hydroxy-1-phenyl-ethyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 349663-64-5
Naphthalene-1-carboxylic acid (R)-2-[benzyl-(naphthalene-1-carbonyl)-amino]-2-phenyl-ethyl ester

: 349663-29-2
Naphthalene-1-carboxylic acid benzyl-((R)-2-hydroxy-1-phenyl-ethyl)-amide

Guidance literature:: With potassium carbonate; In methanol;
DOI:10.1016/S0040-4039(01)00502-0

Reference yield:

: 875-74-1
(R)-phenylglycine

: 349663-29-2
Naphthalene-1-carboxylic acid benzyl-((R)-2-hydroxy-1-phenyl-ethyl)-amide

Guidance literature:: Multi-step reaction with 4 steps

1: 50 percent / NaBH₄; H₂SO₄ / tetrahydrofuran

2: 66 percent / DBU / toluene

3: Et₃N / CH₂Cl₂

4: 79 percent / K₂CO₃ / methanol

With sodium tetrahydroborate; sulfuric acid; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1016/S0040-4039(01)00502-0

Reference yield:

: 56613-80-0
D-2-phenylglycinol

: 349663-29-2
Naphthalene-1-carboxylic acid benzyl-((R)-2-hydroxy-1-phenyl-ethyl)-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 66 percent / DBU / toluene

2: Et₃N / CH₂Cl₂

3: 79 percent / K₂CO₃ / methanol

With potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In methanol; dichloromethane; toluene;
DOI:10.1016/S0040-4039(01)00502-0