C₂₂H₂₄F₆N₂O

Base Information

Chemical Name:C₂₂H₂₄F₆N₂O
CAS No.:552291-47-1
Molecular Formula:C₂₂H₂₄F₆N₂O
Molecular Weight:446.436
Hs Code.:

C<sub>22</sub>H<sub>24</sub>F<sub>6</sub>N<sub>2</sub>O

Synonyms:C₂₂H₂₄F₆N₂O

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Chemical Property of C₂₂H₂₄F₆N₂O

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Technology Process of C₂₂H₂₄F₆N₂O

There total 6 articles about C₂₂H₂₄F₆N₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 530440-44-9
C₂₂H₂₂F₆N₂O₂

: 552291-47-1
C₂₂H₂₄F₆N₂O

Guidance literature:: With aluminum (III) chloride; lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; at -78 - 23 ℃;

Reference yield:

: C₂₂H₂₃F₆NO₂S

: 552291-47-1
C₂₂H₂₄F₆N₂O

Guidance literature:: Multi-step reaction with 7 steps

1.1: diethyl ether; dichloromethane / 3 h / -78 °C

2.1: ozone / dichloromethane / 0.17 h / -78 °C

2.2: Inert atmosphere

3.1: caesium carbonate / N,N-dimethyl-formamide / 3 h / 23 °C

4.1: palladium 10% on activated carbon; hydrogen / ethanol / 24 h / Inert atmosphere

5.1: hydrogenchloride / methanol; 1,4-dioxane / 3.5 h / 0 - 23 °C

6.1: potassium carbonate / methanol / 0.5 h

7.1: aluminum (III) chloride; lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / -78 - 23 °C

With hydrogenchloride; aluminum (III) chloride; lithium aluminium tetrahydride; palladium 10% on activated carbon; hydrogen; potassium carbonate; caesium carbonate; ozone; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: C₃₂H₄₂F₆N₂O₆S

: 552291-47-1
C₂₂H₂₄F₆N₂O

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / methanol; 1,4-dioxane / 3.5 h / 0 - 23 °C

2: potassium carbonate / methanol / 0.5 h

3: aluminum (III) chloride; lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / -78 - 23 °C

With hydrogenchloride; aluminum (III) chloride; lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether;