12b-benzyl-2,3-dimethoxy-5,6,8,12b-tetrahydroisoindolo[1,2-a]isoquinoline

Base Information

Chemical Name:12b-benzyl-2,3-dimethoxy-5,6,8,12b-tetrahydroisoindolo[1,2-a]isoquinoline
CAS No.:26478-14-8
Molecular Formula:C₂₅H₂₅NO₂
Molecular Weight:371.479
Hs Code.:

Synonyms:12b-benzyl-2,3-dimethoxy-5,6,8,12b-tetrahydroisoindolo[1,2-a]isoquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 12b-benzyl-2,3-dimethoxy-5,6,8,12b-tetrahydroisoindolo[1,2-a]isoquinoline

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Technology Process of 12b-benzyl-2,3-dimethoxy-5,6,8,12b-tetrahydroisoindolo[1,2-a]isoquinoline

There total 3 articles about 12b-benzyl-2,3-dimethoxy-5,6,8,12b-tetrahydroisoindolo[1,2-a]isoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 26478-13-7
12b-benzyl-2,3-dimethoxy-5,12b-dihydroisoindolo[1,2-a]isoquinolin-8(6H)-one

: 26478-14-8
12b-benzyl-2,3-dimethoxy-5,6,8,12b-tetrahydroisoindolo[1,2-a]isoquinoline

Guidance literature:: With aluminum (III) chloride; lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 30 ℃; for 12h;
DOI:10.1039/d1ob01206a

Reference yield:

: 120-20-7
2-(3,4-dimethoxyphenyl)-ethylamine

: 26478-14-8
12b-benzyl-2,3-dimethoxy-5,6,8,12b-tetrahydroisoindolo[1,2-a]isoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / toluene / 12 h / Reflux

2: lithium aluminium tetrahydride; aluminum (III) chloride / tetrahydrofuran / 12 h / 0 - 30 °C

With aluminum (III) chloride; lithium aluminium tetrahydride; toluene-4-sulfonic acid; In tetrahydrofuran; toluene;
DOI:10.1039/d1ob01206a