Technology Process of 3,8-bis(3,4-dimethylphenyl)-2,9-diphenyl-1,10-phenanthroline
There total 6 articles about 3,8-bis(3,4-dimethylphenyl)-2,9-diphenyl-1,10-phenanthroline which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); potassium carbonate;
In
N,N-dimethyl-formamide; toluene;
at 120 ℃;
for 20h;
Inert atmosphere;
DOI:10.1039/c2ob27325j
- Guidance literature:
-
Multi-step reaction with 3 steps
1: palladium(II) trifluoroacetate; silver carbonate; Trimethylacetic acid / 48 h / 20 - 130 °C / Inert atmosphere; Schlenk technique
2: trichlorophosphate; phosphorus pentachloride / 12 h / 120 °C / Inert atmosphere
3: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; N,N-dimethyl-formamide / 20 h / 120 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); palladium(II) trifluoroacetate; phosphorus pentachloride; potassium carbonate; silver carbonate; trichlorophosphate; Trimethylacetic acid;
In
N,N-dimethyl-formamide; toluene;
3: |Suzuki Coupling;
DOI:10.1039/c2ob27325j
- Guidance literature:
-
Multi-step reaction with 2 steps
1: trichlorophosphate; phosphorus pentachloride / 12 h / 120 °C / Inert atmosphere
2: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; N,N-dimethyl-formamide / 20 h / 120 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); phosphorus pentachloride; potassium carbonate; trichlorophosphate;
In
N,N-dimethyl-formamide; toluene;
2: |Suzuki Coupling;
DOI:10.1039/c2ob27325j
