C₂₀H₁₄Cl₃NO₃

Base Information

Chemical Name:C₂₀H₁₄Cl₃NO₃
CAS No.:937056-37-6
Molecular Formula:C₂₀H₁₄Cl₃NO₃
Molecular Weight:422.695
Hs Code.:

C<sub>20</sub>H<sub>14</sub>Cl<sub>3</sub>NO<sub>3</sub>

Synonyms:C₂₀H₁₄Cl₃NO₃

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Chemical Property of C₂₀H₁₄Cl₃NO₃

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Technology Process of C₂₀H₁₄Cl₃NO₃

There total 7 articles about C₂₀H₁₄Cl₃NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 937056-36-5
C₂₁H₁₆Cl₃NO₃

: 937056-37-6
C₂₀H₁₄Cl₃NO₃

Guidance literature:: C₂₁H₁₆Cl₃NO₃; With sodium hydroxide; In tetrahydrofuran; methanol; water; at 20 ℃;

With citric acid; In chloroform; water;
DOI:10.1016/j.bmc.2012.02.054

Reference yield:

: [5-chloro-2-(1H-pyrrol-1-yl)phenyl](2,3-dichlorophenyl)methanone

: 937056-37-6
C₂₀H₁₄Cl₃NO₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: trichlorophosphate / dichloromethane / Cooling with ice

1.2: 20 °C / Cooling with ice

2.1: toluene / 7 h / 100 °C

3.1: sodium tetrahydroborate / methanol / 20 °C

4.1: trifluoroacetic acid / dichloromethane / 8 h / 20 °C

5.1: sodium hydroxide / tetrahydrofuran; methanol; water / 20 °C

With sodium tetrahydroborate; trifluoroacetic acid; sodium hydroxide; trichlorophosphate; In tetrahydrofuran; methanol; dichloromethane; water; toluene; 1.1: Vilsmeier reaction / 1.2: Vilsmeier reaction / 2.1: Wittig reaction / 4.1: Michael reaction;
DOI:10.1016/j.bmc.2012.02.054

Reference yield:

: C₂₁H₁₆Cl₃NO₃

: 937056-37-6
C₂₀H₁₄Cl₃NO₃

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 8 h / 20 °C

2: sodium hydroxide / tetrahydrofuran; methanol; water / 20 °C

With trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; 1: Michael reaction;
DOI:10.1016/j.bmc.2012.02.054