C₂₂H₃₀O₂Si

Base Information

Chemical Name:C₂₂H₃₀O₂Si
CAS No.:1322574-63-9
Molecular Formula:C₂₂H₃₀O₂Si
Molecular Weight:354.565
Hs Code.:

C<sub>22</sub>H<sub>30</sub>O<sub>2</sub>Si

Synonyms:C₂₂H₃₀O₂Si

Suppliers and Price of C₂₂H₃₀O₂Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₂H₃₀O₂Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₂H₃₀O₂Si

There total 1 articles about C₂₂H₃₀O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1197349-14-6
C₂₄H₃₂O₃Si

: 1322574-63-9
C₂₂H₃₀O₂Si

Guidance literature:: C₂₄H₃₂O₃Si; With diisobutylaluminium hydride; In dichloromethane; toluene; at -78 ℃; for 1h; Inert atmosphere;

With water; rochelle salt; In dichloromethane; toluene; at -78 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tet.2011.06.025

Reference yield: 92.0%

: 1322574-63-9
C₂₂H₃₀O₂Si

: 1322574-47-9
(S,E)-4-((tert-butyldiphenylsilyl)oxy)-3-methylpent-2-enal

Guidance literature:: C₂₂H₃₀O₂Si; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 1h; Inert atmosphere;

With triethylamine; In dichloromethane; at -78 - 20 ℃; for 0.666667h; Inert atmosphere;
DOI:10.1016/j.tet.2011.06.025

Reference yield:

: 1322574-63-9
C₂₂H₃₀O₂Si

: C₃₈H₆₄O₅Si₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1 h / -78 °C / Inert atmosphere

1.2: 0.67 h / -78 - 20 °C / Inert atmosphere

2.1: (2R,5R)-(+)-2-tert-butyl-3-methyl-5-benzyl-4-imidazolidinone; diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; trifluoroacetic acid / chloroform / 72 h / -30 °C / Inert atmosphere

3.1: toluene / 3 h / -78 °C / Inert atmosphere; Molecular sieve

3.2: 2 h / -78 - 20 °C / Inert atmosphere

4.1: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 0 - 40 °C / Inert atmosphere

5.1: dimethylsulfide borane complex / tetrahydrofuran / 6 h / 0 - 20 °C / Inert atmosphere

5.2: 2 h / 0 - 20 °C / Inert atmosphere

6.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 19 h / 0 - 20 °C / Inert atmosphere

7.1: ammonium molybdate tetrahydrate; dihydrogen peroxide / ethanol; water / 24 h / 20 °C / Inert atmosphere

8.1: lithium hexamethyldisilazane / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; N,N-dimethyl-formamide / 0.17 h / -40 °C / Inert atmosphere

8.2: 24 h / -40 - 20 °C / Inert atmosphere

9.1: pyridine; pyridine hydrogenfluoride / tetrahydrofuran / 72 h / 20 °C / Inert atmosphere

With pyridine; (2R,5R)-(+)-2-tert-butyl-3-methyl-5-benzyl-4-imidazolidinone; oxalyl dichloride; ammonium molybdate tetrahydrate; di-isopropyl azodicarboxylate; dimethylsulfide borane complex; diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; dihydrogen peroxide; tetra-(n-butyl)ammonium iodide; pyridine hydrogenfluoride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; triphenylphosphine; trifluoroacetic acid; lithium hexamethyldisilazane; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; toluene; 1.1: Swern oxidation / 1.2: Swern oxidation / 3.1: Roush crotylation / 6.1: Mitsunobu reaction / 8.2: Julia-Kocienski olefinaton;
DOI:10.1016/j.tet.2011.06.025