(κ²-2,11-dithia[3.3](2,6)pyridinophane)PdMeBr

Base Information

• Chemical Name: (κ²-2,11-dithia[3.3](2,6)pyridinophane)PdMeBr
• CAS No.: 1438401-89-8
• Molecular Formula: C₁₅H₁₇BrN₂PdS₂
• Molecular Weight: 475.769

Synonyms:(κ²-2,11-dithia[3.3](2,6)pyridinophane)PdMeBr

Chemical Property of (κ²-2,11-dithia[3.3](2,6)pyridinophane)PdMeBr

Chemical Property:

Purity/Quality:

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Technology Process of (κ²-2,11-dithia[3.3](2,6)pyridinophane)PdMeBr

There total 1 articles about (κ²-2,11-dithia[3.3](2,6)pyridinophane)PdMeBr which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[(κ4-2,11-dithia[3.3](2,6)pyridinophane)PdMe2](PF6)2*acetone + tetrabutylammomium bromide (1643-19-2) → methyl bromide (74-83-9) + (κ2-2,11-dithia[3.3](2,6)pyridinophane)PdMeBr (1438401-89-8)

Guidance literature:

In [⁽²⁾H₆]acetone; for 0.0833333h; Inert atmosphere; Schlenk technique; Glovebox;

DOI:10.1021/om400286j

Reference yield:

(κ2-2,11-dithia[3.3](2,6)pyridinophane)PdMeBr (1438401-89-8) → methyl bromide (74-83-9) + [(2,11-dithia[3.3](2,6)pyridinophane)PdBr]+ + [(2,11-dithia[3.3](2,6)pyridinophane)PdIIMe]+

Guidance literature:

With acetylferrocenium tetrafluoroborate; In [⁽²⁾H₆]acetone; at 20 ℃; for 2h; Reagent/catalyst; Temperature; Time; Inert atmosphere; Schlenk technique; Glovebox;

DOI:10.1021/om400286j

Reference yield:

[13C]methyl iodide (4227-95-6) + (κ2-2,11-dithia[3.3](2,6)pyridinophane)PdMeBr (1438401-89-8) → methyl bromide-13C (51624-21-6) + (2,11-dithia[3.3](2,6)pyridinophane)PdMeI

Guidance literature:

In [⁽²⁾H₆]acetone; at 20 ℃; for 18h; Reagent/catalyst; Inert atmosphere; Schlenk technique; Glovebox;

DOI:10.1021/om400286j

upstream raw materials:

tetrabutylammomium bromide

Downstream raw materials:

methyl bromide

methyl bromide-13C

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