4-{[(4-dodecyloxyphenyl)carbonyl]oxy}phenyl thiophene-2-carboxylate

Base Information

Chemical Name:4-{[(4-dodecyloxyphenyl)carbonyl]oxy}phenyl thiophene-2-carboxylate
CAS No.:1459717-62-4
Molecular Formula:C₃₀H₃₆O₅S
Molecular Weight:508.679
Hs Code.:

Synonyms:4-{[(4-dodecyloxyphenyl)carbonyl]oxy}phenyl thiophene-2-carboxylate

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Chemical Property of 4-{[(4-dodecyloxyphenyl)carbonyl]oxy}phenyl thiophene-2-carboxylate

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Technology Process of 4-{[(4-dodecyloxyphenyl)carbonyl]oxy}phenyl thiophene-2-carboxylate

There total 12 articles about 4-{[(4-dodecyloxyphenyl)carbonyl]oxy}phenyl thiophene-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.9%

: 5271-67-0
2-Thiophenecarbonyl chloride

: 123436-82-8
4-(hydroxy)phenyl 4-(dodecyloxy)benzoate

: 1459717-62-4
4-{[(4-dodecyloxyphenyl)carbonyl]oxy}phenyl thiophene-2-carboxylate

Guidance literature:: With triethylamine; In butanone; at 0 ℃; for 5.75h;
DOI:10.1080/15421406.2013.790635

Reference yield:

: 99-76-3,156291-94-0
methyl 4-hydroxylbenzoate

: 1459717-62-4
4-{[(4-dodecyloxyphenyl)carbonyl]oxy}phenyl thiophene-2-carboxylate

Guidance literature:: Multi-step reaction with 6 steps

1: potassium carbonate / N,N-dimethyl-formamide / 4.5 h / 90 °C

2: potassium hydroxide / ethanol; water / 2 h / Reflux

3: thionyl chloride / N,N-dimethyl-formamide / 0.5 h / 0 °C / Reflux

4: triethylamine / butanone / 4.5 h / 0 °C / Cooling with ice

5: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 20 °C

6: triethylamine / butanone / 5.75 h / 0 °C

With thionyl chloride; palladium 10% on activated carbon; hydrogen; potassium carbonate; triethylamine; potassium hydroxide; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; butanone;
DOI:10.1080/15421406.2013.790635

Reference yield:

: 40654-49-7
methyl 4-(dodecyloxy)benzoate

: 1459717-62-4
4-{[(4-dodecyloxyphenyl)carbonyl]oxy}phenyl thiophene-2-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: potassium hydroxide / ethanol; water / 2 h / Reflux

2: thionyl chloride / N,N-dimethyl-formamide / 0.5 h / 0 °C / Reflux

3: triethylamine / butanone / 4.5 h / 0 °C / Cooling with ice

4: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 20 °C

5: triethylamine / butanone / 5.75 h / 0 °C

With thionyl chloride; palladium 10% on activated carbon; hydrogen; triethylamine; potassium hydroxide; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; butanone;
DOI:10.1080/15421406.2013.790635