Technology Process of C68H70Br8N4
There total 4 articles about C68H70Br8N4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C36H48N2O4;
With
trichlorophosphate;
In
N,N-dimethyl-formamide;
at 70 ℃;
for 2h;
With
titanium tetrachloride; copper(l) chloride; zinc;
In
tetrahydrofuran;
for 4h;
Reflux;
With
hydrogen bromide;
In
acetic acid;
at 20 ℃;
for 168h;
DOI:10.1002/adma.201203459
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 72 h / 20 °C
2.1: Iodine monochloride; sodium acetate / acetic acid / 80 °C
3.1: copper / toluene / 72 h / Reflux
4.1: sodium hydroxide; ethylene glycol / 1 h / 190 °C
5.1: trichlorophosphate / N,N-dimethyl-formamide / 2 h / 70 °C
5.2: 4 h / Reflux
5.3: 168 h / 20 °C
With
sodium acetate; Iodine monochloride; copper; ethylene glycol; 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium hydroxide; trichlorophosphate;
In
tetrahydrofuran; acetic acid; N,N-dimethyl-formamide; toluene;
3.1: |Ullmann Condensation;
DOI:10.1002/adma.201203459
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: Iodine monochloride; sodium acetate / acetic acid / 80 °C
2.1: copper / toluene / 72 h / Reflux
3.1: sodium hydroxide; ethylene glycol / 1 h / 190 °C
4.1: trichlorophosphate / N,N-dimethyl-formamide / 2 h / 70 °C
4.2: 4 h / Reflux
4.3: 168 h / 20 °C
With
sodium acetate; Iodine monochloride; copper; ethylene glycol; sodium hydroxide; trichlorophosphate;
In
acetic acid; N,N-dimethyl-formamide; toluene;
2.1: |Ullmann Condensation;
DOI:10.1002/adma.201203459
