Technology Process of C36H54O3
There total 5 articles about C36H54O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine;
at -20 ℃;
for 1h;
With
chloroformic acid ethyl ester;
In
tetrahydrofuran;
at -20 - 20 ℃;
for 3h;
12-Phenyldodecanoic Acid;
With
triethylamine;
In
tetrahydrofuran;
at -20 - 20 ℃;
DOI:10.1016/S0040-4039(02)00758-X
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: AlCl3 / 13 h / 4 - 20 °C
2.1: aq. HCl
3.1: NH2NH2; KOH / ethane-1,2-diol / 4 h / Heating
3.2: 70 percent / H3O(+) / H2O
4.1: Et3N / 1 h / -20 °C
4.2: ClCO2Et / tetrahydrofuran / 3 h / -20 - 20 °C
4.3: Et3N / tetrahydrofuran / -20 - 20 °C
With
hydrogenchloride; potassium hydroxide; aluminium trichloride; triethylamine; hydrazine;
In
ethylene glycol;
1.1: Friedel-Crafts reaction / 3.1: Huang-Minlon reaction;
DOI:10.1016/S0040-4039(02)00758-X
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: NH2NH2; KOH / ethane-1,2-diol / 4 h / Heating
1.2: 70 percent / H3O(+) / H2O
2.1: Et3N / 1 h / -20 °C
2.2: ClCO2Et / tetrahydrofuran / 3 h / -20 - 20 °C
2.3: Et3N / tetrahydrofuran / -20 - 20 °C
With
potassium hydroxide; triethylamine; hydrazine;
In
ethylene glycol;
1.1: Huang-Minlon reaction;
DOI:10.1016/S0040-4039(02)00758-X
