benzyl 2-aminocarbonyl-3,3-diethoxy-5-methyl-2H-1,2,3λ⁵-diazaphosphole-4-carboxylate

Base Information

• Chemical Name: benzyl 2-aminocarbonyl-3,3-diethoxy-5-methyl-2H-1,2,3λ⁵-diazaphosphole-4-carboxylate
• CAS No.: 852879-20-0
• Molecular Formula: C₁₆H₂₂N₃O₅P
• Molecular Weight: 367.342

Synonyms:benzyl 2-aminocarbonyl-3,3-diethoxy-5-methyl-2H-1,2,3λ⁵-diazaphosphole-4-carboxylate

Chemical Property of benzyl 2-aminocarbonyl-3,3-diethoxy-5-methyl-2H-1,2,3λ⁵-diazaphosphole-4-carboxylate

Chemical Property:

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Technology Process of benzyl 2-aminocarbonyl-3,3-diethoxy-5-methyl-2H-1,2,3λ⁵-diazaphosphole-4-carboxylate

There total 1 articles about benzyl 2-aminocarbonyl-3,3-diethoxy-5-methyl-2H-1,2,3λ⁵-diazaphosphole-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

C12H13N3O3 + triethyl phosphite (122-52-1) → benzyl 2-aminocarbonyl-3,3-diethoxy-5-methyl-2H-1,2,3λ5-diazaphosphole-4-carboxylate (852879-20-0)

Guidance literature:

at 20 ℃; for 5.5h;

DOI:10.1021/jo050242n

Reference yield: 95.0%

benzyl 2-aminocarbonyl-3,3-diethoxy-5-methyl-2H-1,2,3λ5-diazaphosphole-4-carboxylate (852879-20-0) → benzyl 3-[(E)-2-(aminocarbonyl)hydrazono]-2-(diethoxyphosphoryl)butanoate (852879-28-8)

Guidance literature:

In tetrahydrofuran; water; at 20 ℃; for 24h;

DOI:10.1021/jo050242n

Reference yield:

benzyl 2-aminocarbonyl-3,3-diethoxy-5-methyl-2H-1,2,3λ5-diazaphosphole-4-carboxylate (852879-20-0) → benzyl 2-(diethoxyphosphoryl)-2-(1,2,3-thiadiazol-4-yl)acetate

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / tetrahydrofuran; H₂O / 24 h / 20 °C

2: 71 percent / thionyl chloride / 1 h / 20 °C

With thionyl chloride; In tetrahydrofuran; water;

DOI:10.1021/jo050242n

upstream raw materials:

triethyl phosphite

Downstream raw materials:

benzyl 3-[(E)-2-(aminocarbonyl)hydrazono]-2-(diethoxyphosphoryl)butanoate

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