(Z)-1-(3-chlorophenyl)-3-methoxy-3-oxoprop-1-en-1-amine hydrochloride

Base Information

Chemical Name:(Z)-1-(3-chlorophenyl)-3-methoxy-3-oxoprop-1-en-1-amine hydrochloride
CAS No.:1245606-57-8
Molecular Formula:C₁₀H₁₀ClNO₂*ClH
Molecular Weight:248.109
Hs Code.:

Synonyms:(Z)-1-(3-chlorophenyl)-3-methoxy-3-oxoprop-1-en-1-amine hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-1-(3-chlorophenyl)-3-methoxy-3-oxoprop-1-en-1-amine hydrochloride

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Technology Process of (Z)-1-(3-chlorophenyl)-3-methoxy-3-oxoprop-1-en-1-amine hydrochloride

There total 1 articles about (Z)-1-(3-chlorophenyl)-3-methoxy-3-oxoprop-1-en-1-amine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 632327-19-6
methyl 3-(3-chlorophenyl)-3-oxopropanoate

: 1245606-57-8
(Z)-1-(3-chlorophenyl)-3-methoxy-3-oxoprop-1-en-1-amine hydrochloride

Guidance literature:: methyl 3-(3-chlorophenyl)-3-oxopropanoate; With ammonium acetate; In methanol; for 12h; Inert atmosphere; Reflux;

With hydrogenchloride; In diethyl ether; tert-butyl methyl ether; for 0.5h; Inert atmosphere;
DOI:10.1021/ja105674y

Reference yield: 90.0%

: 1245606-57-8
(Z)-1-(3-chlorophenyl)-3-methoxy-3-oxoprop-1-en-1-amine hydrochloride

: 1245606-65-8
(S)-1-(3-chlorophenyl)-3-methoxy-3-oxopropan-1-amine hydrochloride

Guidance literature:: With bis(1,5-cyclooctadiene)diiridium(I) dichloride; 1,1'-bis[(S)-4,5-dihydro-3H-binaphtho[2,1-c:1',2'-e]phosphino]ferrocene; hydrogen; In methanol; dichloromethane; at 20 ℃; for 12h; under 38002.6 Torr; optical yield given as %ee; enantioselective reaction;
DOI:10.1021/ja105674y