cis-5,6-Dihydrodibenzo<1,2>diazocine

Base Information

Chemical Name:cis-5,6-Dihydrodibenzo<1,2>diazocine
CAS No.:21372-42-9
Molecular Formula:C₁₄H₁₂N₂
Molecular Weight:208.263
Hs Code.:

cis-5,6-Dihydrodibenzo<c,g><1,2>diazocine

Synonyms:cis-5,6-Dihydrodibenzo<1,2>diazocine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cis-5,6-Dihydrodibenzo<1,2>diazocine

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Technology Process of cis-5,6-Dihydrodibenzo<1,2>diazocine

There total 2 articles about cis-5,6-Dihydrodibenzo<1,2>diazocine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 34124-14-6
2,2'-ethylenedianiline

cis-5,6-Dihydrodibenzo<1,2>diazocine: 21372-42-9
cis-5,6-Dihydrodibenzo<1,2>diazocine

: 40754-26-5
5,6-dihydrodibenzo-1,2-diazocine N-oxide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetic acid; for 13h;
DOI:10.1021/jacs.9b08794

Reference yield: 42.0%

: 85071-27-8
2-nitrobenzyl thiocyanate

cis-5,6-Dihydrodibenzo<1,2>diazocine: 21372-42-9
cis-5,6-Dihydrodibenzo<1,2>diazocine

: 956-31-0,51284-68-5,116723-89-8
N,N'-Di-o-tolyl-diazene N-oxide

: 40754-26-5
5,6-dihydrodibenzo-1,2-diazocine N-oxide

Guidance literature:: Electrolytic reduction in weakly alkaline medium;

Reference yield: 89.0%

cis-5,6-Dihydrodibenzo<1,2>diazocine: 21372-42-9
cis-5,6-Dihydrodibenzo<1,2>diazocine

: 34124-14-6
2,2'-ethylenedianiline

Guidance literature:: With pyridine; palladium on activated charcoal; hydrogen; In methanol; at 20 ℃; for 0.25h; under 760.051 Torr; Green chemistry;
DOI:10.1039/d1ob00850a