3-nitro-4-thiocyanatoaniline

Base Information

• Chemical Name: 3-nitro-4-thiocyanatoaniline
• CAS No.: 23153-15-3
• Molecular Formula: C₇H₅N₃O₂S
• Molecular Weight: 195.202
• Mol file: 23153-15-3.mol

Synonyms:3-nitro-4-thiocyanatoaniline

Chemical Property of 3-nitro-4-thiocyanatoaniline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-nitro-4-thiocyanatoaniline

There total 3 articles about 3-nitro-4-thiocyanatoaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

ammonium thiocyanate (1147550-11-5) + 3-nitro-aniline (99-09-2) → 3-nitro-4-thiocyanatoaniline (23153-15-3)

Guidance literature:

With iron(III) chloride; In dichloromethane; at 20 ℃; for 4h;

DOI:10.1055/s-2005-861852

Reference yield: 8.0%

3-nitro-aniline (99-09-2) + 1-methyl-3-phenyl-2,4-dioxo-1,2,3,4-tetrahydroquinolin-3-yl thiocyanate (521980-39-2) → 3-nitro-4-thiocyanatoaniline (23153-15-3)

Guidance literature:

In chloroform; for 40h; Heating;

DOI:10.1002/jhet.5570400501

Reference yield:

→ 3-nitro-4-thiocyanatoaniline (23153-15-3)

Guidance literature:

3-Nitro-anilin, NH4-Thiocyanat, Eg., N-Brom-acetamid;

upstream raw materials:

3-nitro-aniline

1-methyl-3-phenyl-2,4-dioxo-1,2,3,4-tetrahydroquinolin-3-yl thiocyanate

ammonium thiocyanate

Downstream raw materials:

benzo[d]thiazole-2,5-diamine

4-chloro-2-nitro-phenyl thiocyanate