[CH₂C₉H₆NPd(C(CF₃)C(CF₃)C(CF₃)C(CF₃))PdCH(Si(CH₃)3)C₆H₄N(CH₃)2]

Base Information

• Chemical Name: [CH₂C₉H₆NPd(C(CF₃)C(CF₃)C(CF₃)C(CF₃))PdCH(Si(CH₃)3)C₆H₄N(CH₃)2]
• CAS No.: 93184-78-2
• Molecular Formula: C₃₀H₂₈F₁₂N₂Pd₂Si
• Molecular Weight: 885.472
• Mol file: 93184-78-2.mol

Synonyms:[CH₂C₉H₆NPd(C(CF₃)C(CF₃)C(CF₃)C(CF₃))PdCH(Si(CH₃)3)C₆H₄N(CH₃)2]

Chemical Property of [CH₂C₉H₆NPd(C(CF₃)C(CF₃)C(CF₃)C(CF₃))PdCH(Si(CH₃)3)C₆H₄N(CH₃)2]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [CH₂C₉H₆NPd(C(CF₃)C(CF₃)C(CF₃)C(CF₃))PdCH(Si(CH₃)3)C₆H₄N(CH₃)2]

There total 2 articles about [CH₂C₉H₆NPd(C(CF₃)C(CF₃)C(CF₃)C(CF₃))PdCH(Si(CH₃)3)C₆H₄N(CH₃)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

[Pd(CH(Si(CH3)3)C6H4N(CH3)2)(CH2C9H6N)] (93184-76-0) + hexafluoro-2-butyne (692-50-2) → [CH2C9H6NPd(C(CF3)C(CF3)C(CF3)C(CF3))PdCH(Si(CH3)3)C6H4N(CH3)2] (93184-78-2) + C9H6NCH2CH(Si(CH3)3)C6H4N(CH3)2 (93184-80-6)

Guidance literature:

In toluene; CF3C2CF3(excess), toluene, room temp.;

DOI:10.1021/ja00337a076

Reference yield:

2-(dimethylamino)-α-lithio-{α-(trimethylsilyl)methyl}benzene + [PdCl(CH2C9H6N)]2 (28377-73-3) → [CH2C9H6NPd(C(CF3)C(CF3)C(CF3)C(CF3))PdCH(Si(CH3)3)C6H4N(CH3)2] (93184-78-2) + C9H6NCH2CH(Si(CH3)3)C6H4N(CH3)2 (93184-80-6)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether

2: toluene

In diethyl ether; toluene;

DOI:10.1021/ja00337a076

upstream raw materials:

[Pd(CH(Si(CH₃)3)C₆H₄N(CH₃)2)(CH₂C₉H₆N)]

hexafluoro-2-butyne

[PdCl(CH₂C₉H₆N)]2