d-menthyl diazoacetate

Base Information

Chemical Name:d-menthyl diazoacetate
CAS No.:65437-23-2
Molecular Formula:C₁₂H₂₀N₂O₂
Molecular Weight:224.303
Hs Code.:

Synonyms:d-menthyl diazoacetate

Suppliers and Price of d-menthyl diazoacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of d-menthyl diazoacetate

Chemical Property:

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Technology Process of d-menthyl diazoacetate

There total 5 articles about d-menthyl diazoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 120143-37-5
(1S,3S,4R)-menthyl glycinate

: 65437-23-2
d-menthyl diazoacetate

Guidance literature:: With acetic acid; isopentyl nitrite; In chloroform; for 3.5h; Heating;
DOI:10.1002/hlca.19880710621

Reference yield:

: 146143-51-3
d-(+)-menthyl diazoacetoacetate

: 65437-23-2
d-menthyl diazoacetate

Guidance literature:: With lithium hydroxide monohydrate; In water; acetonitrile; at 20 ℃; for 6h; Inert atmosphere;
DOI:10.1021/jacs.7b04756

Reference yield:

: 15356-60-2
(1S,2R,5S)-(+)-menthol

: 65437-23-2
d-menthyl diazoacetate

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / pyridine / diethyl ether / 4 h / 23 °C

2: 88 percent / aq.NH₃ / dimethylformamide / 24 h / 23 °C

3: 62 percent / isopentyl nitrite, AcOH / CHCl₃ / 3.5 h / Heating

With pyridine; ammonium hydroxide; acetic acid; isopentyl nitrite; In diethyl ether; chloroform; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19880710621