N-[1-fluoromethyl-2-(2,4,6-trichlorophenyl)-ethyl]-O-methyl-hydroxylamine

Base Information

Chemical Name:N-[1-fluoromethyl-2-(2,4,6-trichlorophenyl)-ethyl]-O-methyl-hydroxylamine
CAS No.:1351601-06-3
Molecular Formula:C₁₀H₁₁Cl₃FNO
Molecular Weight:286.561
Hs Code.:

Synonyms:N-[1-fluoromethyl-2-(2,4,6-trichlorophenyl)-ethyl]-O-methyl-hydroxylamine

Suppliers and Price of N-[1-fluoromethyl-2-(2,4,6-trichlorophenyl)-ethyl]-O-methyl-hydroxylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-[1-fluoromethyl-2-(2,4,6-trichlorophenyl)-ethyl]-O-methyl-hydroxylamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-[1-fluoromethyl-2-(2,4,6-trichlorophenyl)-ethyl]-O-methyl-hydroxylamine

There total 10 articles about N-[1-fluoromethyl-2-(2,4,6-trichlorophenyl)-ethyl]-O-methyl-hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 1351601-21-2
2-methoxyamino-3-(2,4,6-trichlorophenyl)-propan-1-ol

: 1351601-06-3
N-[1-fluoromethyl-2-(2,4,6-trichlorophenyl)-ethyl]-O-methyl-hydroxylamine

Guidance literature:: 2-methoxyamino-3-(2,4,6-trichlorophenyl)-propan-1-ol; With diethylamino-sulfur trifluoride; In dichloromethane; at -16 - 20 ℃; for 2h; Inert atmosphere;

With sodium hydrogencarbonate; In dichloromethane;

Reference yield: 25.0%

: 1351601-20-1
1-fluoro-3-(2,4,6-trichloro-phenyl)-propan-2-one O-methyl-oxime

: 1351601-06-3
N-[1-fluoromethyl-2-(2,4,6-trichlorophenyl)-ethyl]-O-methyl-hydroxylamine

Guidance literature:: 1-fluoro-3-(2,4,6-trichloro-phenyl)-propan-2-one O-methyl-oxime; With sodium cyanoborohydride; acetic acid; at 24 - 35 ℃; for 36h;

With water; sodium hydroxide; pH=14; Cooling with ice;

Reference yield:

: 1351601-16-5
1-hydroxy-3-(2,4,6-trichloro-phenyl)-propan-2-one O-methyl-oxime

: 1351601-06-3
N-[1-fluoromethyl-2-(2,4,6-trichlorophenyl)-ethyl]-O-methyl-hydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: diethylamino-sulfur trifluoride / dichloromethane / 2 h / -20 - 20 °C / Inert atmosphere

2.1: sodium cyanoborohydride; acetic acid / 36 h / 24 - 35 °C

2.2: pH 14 / Cooling with ice

With diethylamino-sulfur trifluoride; sodium cyanoborohydride; acetic acid; In dichloromethane;